Method for preparing Cu-Fe alloy from Cu cuttings and Fe cuttings

A cu-fe, alloy technology, applied in the direction of transportation and packaging, metal processing equipment, etc., can solve the problems of large powder surface area, reduce the conductivity of the alloy, affect the conductivity, etc., to improve the conductivity, improve the mechanical properties, reduce the solid melting effect

Inactive Publication Date: 2020-08-11
INST OF APPLIED PHYSICS JIANGXI ACADEMY OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, Cu-Fe alloys are mainly prepared by conventional melting and casting methods, followed by subsequent deformation processing and heat treatment; during melting and casting, a large amount of Fe elements are usually solid-dissolved in the Cu matrix, which seriously reduces the conductivity of the alloy, and subsequent processing can only cause part of Fe to precipitate. , the remaining solid solution Fe still significantly affects the conductivity
Although Cu-Fe alloy is prepared by hot pressing and sintering of Cu powder and Fe powder, it avoids melting and casting, but the powder has a large surface area and strong activity. During the preparation process, it is inevitable that the electrical conductivity will be affected due to easy oxidation and too many interfaces.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0014] The present embodiment provides the method for preparing Cu-5Fe alloy, comprises the following steps:

[0015] 1. Machining pure Cu and pure Fe: use a lathe to process pure Cu into chips with a size of 6mm×3mm×0.7mm, process pure Fe into chips with a size of 4mm×2mm×0.8mm, and place the two or mixed evenly with a mass ratio of 19:1;

[0016] 2. Press the mixed chips at 750MPa and room temperature for 50s to obtain a cold-pressed ingot;

[0017] 3. The cold-pressed ingot is pressed at 700MPa and 950°C for 60s to obtain a hot-pressed ingot;

[0018] 4. The hot-pressed billet is extruded into rods at 850°C according to the extrusion ratio of 25:1 and the extrusion speed of 0.3mm / s;

[0019] 5. Carry out multi-pass cold drawing of the bar at room temperature until the area shrinkage rate is 99.99%, and obtain the wire;

[0020] 6. Annealing the wire at 200°C to obtain a high-strength and high-conductivity Cu-5Fe alloy.

Embodiment 2

[0022] The present embodiment provides the method for preparing Cu-10Fe alloy, comprises the following steps:

[0023] 1. Machining pure Cu and pure Fe: use a lathe to process pure Cu into scraps with a size of 8mm×2mm×0.3mm, and process pure Fe into scraps with a size of 5mm×1mm×0.5mm. or mixed evenly with a mass ratio of 9:1;

[0024] 2. Press the mixed chips at 800MPa and room temperature for 55s to obtain a cold-pressed ingot;

[0025] 3. The cold-pressed billet is pressed at 750MPa and 950°C for 65s to obtain a hot-pressed billet;

[0026] 4. The hot-pressed billet is extruded into rods at 900°C according to the extrusion ratio of 25:1 and the extrusion speed of 0.2mm / s;

[0027] 5. Carry out multi-pass cold drawing of the bar at room temperature until the area shrinkage rate is 99.99%, and obtain the wire;

[0028] 6. The wire is annealed at 300°C to obtain a high-strength and high-conductivity Cu-10Fe alloy.

Embodiment 3

[0030] The present embodiment provides the method for preparing Cu-15Fe alloy, comprises the following steps:

[0031] 1. Machining pure Cu and pure Fe: use a lathe to process pure Cu into scraps with a size of 10mm×1mm×0.2mm, and process pure Fe into scraps with a size of 6mm×1.5mm×0.3mm. The two are evenly mixed with a mass ratio of 17:3;

[0032] 2. Press the mixed chips at 890MPa and room temperature for 60s to obtain a cold-pressed ingot;

[0033] 3. The cold-pressed ingot is pressed at 750MPa and 1000°C for 70s to obtain a hot-pressed ingot;

[0034] 4. The hot-pressed billet is extruded into rods at 900°C with an extrusion ratio of 36:1 and an extrusion speed of 0.1mm / s;

[0035] 5. Carry out multi-pass cold drawing of the bar at room temperature until the area shrinkage rate is 99.75%, and obtain the wire;

[0036] 6. The wire is annealed at 350°C to obtain a high-strength and high-conductivity Cu-15Fe alloy.

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PUM

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Abstract

The invention provides a method for preparing a Cu-Fe alloy from Cu cuttings and Fe cuttings. The mass ratio of the pure Cu cuttings to the pure Fe cuttings is 4-99:1. The method comprises the steps of uniformly mixing the pure Cu cuttings with the size of (0.1-11) mm*(0.1-4.9) mm*(0.01-1.57) mm and the pure Fe cuttings with the size of (0.1-6.5) mm*(0.1-2.7) mm*(0.01-1.46) mm; pressing the mixedcuttings at 600-890 MPa and indoor temperature for 25-65 s to obtain a cold pressed billet; pressing the cold pressed billet at 650-750 MPa and 900-1000 DEG C for 35-70 s to obtain a hot pressed billet; extruding the hot pressed billet into a bar at the extrusion ratio of 25-36:1 at 800-900 DEG C and extrusion speed of 0.1-0.5 mm / s; conducting multi-pass cold drawing on the bar at indoor temperature to obtain a wire with the percentage of cross-section contraction being 99.75%-99.99%; and finally conducting annealing treatment on the wire at 200-500 DEG C to obtain the high-strength high-conductivity Cu-Fe alloy. According to the Cu-Fe alloy prepared through the method, the melting process is not needed, oxidization and burning loss of a raw material can be effectively avoided, the solid solution rate of Fe in Cu can be greatly reduced, and accordingly, the conductivity of the Cu-Fe alloy is remarkably improved.

Description

technical field [0001] The invention belongs to the field of copper alloys, and relates to a method for preparing Cu-Fe alloys by using chips. Background technique [0002] Copper alloy has good electrical conductivity and mechanical properties, and strong plastic deformation ability. It is a key material in electronics, energy, machinery, ships and other industries. Among them, Cu-Fe alloy is low in cost, easy to smelt and plastically processed, and is used as a high-strength and high-conductivity alloy. It has broad application prospects and has attracted extensive attention from researchers. [0003] At present, Cu-Fe alloys are mainly prepared by conventional melting and casting methods, followed by subsequent deformation processing and heat treatment; during melting and casting, a large amount of Fe elements are usually solid-dissolved in the Cu matrix, which seriously reduces the conductivity of the alloy, and subsequent processing can only cause part of Fe to precipit...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C9/00C22C1/04B22F1/00B22F3/02B22F3/14B22F3/20B22F3/24C22F1/08
CPCC22C9/00C22C1/0425B22F3/02B22F3/14B22F3/20B22F3/24C22F1/08B22F2003/208B22F2003/248B22F1/068
Inventor 郭炜谌昀陈威
Owner INST OF APPLIED PHYSICS JIANGXI ACADEMY OF SCI
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