The invention discloses a preparation method of a CoCrFeNiCuPrx high-entropy
alloy based on H3Pr, and relates to a CoCrFeNiCuPrx high-entropy
alloy. The H3Pr
powder and the high-entropy
alloy are prepared through a direct hydrogenation method and a
powder metallurgy method respectively, and Co, Cr, Fe, Ni and Cu elementary substance
powder and intermediate
hydride H3Pr powder are weighed according to the proportion; and after high-energy mechanical ball milling, the powder is pressed and molded into a small round
ingot, and the small round
ingot is sintered through a vacuum rapid
hot pressing sintering process, so that all elements are fully diffused. According to the preparation method disclosed by the invention, the CoCrFeNiCuPrx high-entropy alloy is prepared on the basis of H3Pr; the problems that the strength and
hardness of the CoCrFeNiCu high-entropy alloy are low and the strength and
hardness of the CoCrFeNiCu high-entropy alloy are not obviously improved by elemental Pr are solved, the
decomposition temperature of H3Pr during heating is lower than the
melting point of
metal Pr, released Pr atoms can enter surrounding high-entropy alloy matrix
crystal lattices only through short-distance
diffusion, segregation of matrix elements and the oxidation tendency of Pr are greatly relieved, and the strength and
hardness of the CoCrFeNiCu high-entropy alloy is improved. And a
microstructure with relatively uniform components is obtained.