Method and mold for preparing microscopic analysis sample of double-layer asphalt diffusion system

A mold and sample technology, which is applied in the field of preparing microscopic analysis samples of double-layer asphalt diffusion system, can solve the problems of analysis sample thickness difference, analysis sample surface unevenness, and influence of mesostructure analysis, etc., to achieve smooth surface, uniform diffusion, The effect of increasing realism

Pending Publication Date: 2020-08-21
INNER MONGOLIA UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the method of studying the mesoscopic observation of the double-layer asphalt diffusion system is mainly to heat the analysis sample to the molten state and drop it on the slide glass, then heat it until it disperses freely, and then cool it for later use; however, this method cannot fully guarantee the quality of the analysis sample. Evenly spread out, resulting in uneven surface of the analysis sample, and at the same time, it is difficult to control the amount of asphalt and it is easy to cause the difference in the thickness of the analysis sample
In response to this problem, the Chinese patent "CN104502168A" discloses a method for preparing asphalt microscopic analysis samples using silica gel molds. The analysis samples are directly added to the prepared single silica gel molds to ensure the uniformity of the analysis samples; Due to the inability to accurately control the amount of asphalt used in the mold, it will affect the subsequent microstructure analysis

Method used

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  • Method and mold for preparing microscopic analysis sample of double-layer asphalt diffusion system
  • Method and mold for preparing microscopic analysis sample of double-layer asphalt diffusion system
  • Method and mold for preparing microscopic analysis sample of double-layer asphalt diffusion system

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Embodiment 1

[0033] Such as Figure 1-5 As shown, this embodiment provides a method for preparing a microscopic analysis sample of a double-layer asphalt diffusion system, including the following steps:

[0034] S1, first heating the old and new asphalt to a fluid state, then injecting them into the upper mold 3 and the lower mold 4 respectively, and cooling, forming the upper sample 6 in the upper mold 3, and forming the lower sample 5 in the lower mold, wherein the upper Sample 6 is new asphalt, and lower sample 5 is old asphalt.

[0035] S2, first superimposing and merging the upper mold 3 and the lower mold 5, so that the upper sample 6 and the lower sample 5 are in contact, and then heating, so that the upper sample 6 and the lower sample 5 are fully diffused;

[0036] S3, first cooling the upper mold 3 and the lower mold 4 together, then removing the upper mold 3 and the lower mold 4, placing the double-layer analysis sample 7 composed of the upper sample 6 and the lower sample 5 on...

Embodiment 2

[0042] Such as Figure 1-5As shown, based on the method for preparing the microscopic analysis sample of the double-layer asphalt diffusion system in Example 1, this embodiment provides a mold for preparing the microscopic analysis sample of the double-layer asphalt diffusion system, including the upper structure, the lower structure and the double-layer fixed mold 8; wherein, the upper structure includes an upper mold 3 and a cover plate; the lower structure includes a lower mold 4, two lower fixed molds 1 and a glass slide 8; The hole I and the through hole II are coaxial, and the lower fixed mold 1 is provided with a slot I for installing the lower mold, and a through slot I is provided close to the slot I for the free insertion of the glass slide 8; the double-layer fixed mold 2 There is a card slot II on the top, and the card slot II is used to install the superimposed and combined upper mold 3 and the lower mold 4, and a through slot II for slide glass 8 to be freely ins...

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Abstract

The invention discloses a method and mold for preparing a microscopic analysis sample of a double-layer asphalt diffusion system. The method comprises the following steps: S1, respectively heating newasphalt and old asphalt to a flowing state, respectively injecting the processed new asphalt and old asphalt into an upper-layer mold and a lower-layer mold, and performing cooling to obtain an upper-layer sample and a lower-layer sample; S2, superposing and combining the upper-layer mold and the lower-layer mold to enable the upper-layer sample and the lower-layer sample to be in contact, and then performing heating to enable the upper-layer sample and the lower-layer sample to be fully diffused; S3, cooling and demolding the upper-layer mold and the lower-layer mold, placing a double-layeranalysis sample consisting of the upper-layer sample and the lower-layer sample on a glass slide, performing heating, taking out the product, cooling and storing the product; and S4, performing asphalt microscopic test observation on the cooled and stored double-layer analysis sample. With the method, a technical problem that the specification, the shape and the quality of an analysis sample cannot be controlled in the preparation and forming process is effectively solved, the use amount of asphalt can be effectively controlled, and the authenticity of subsequent asphalt and asphalt mixture material and mechanical property evaluation is improved.

Description

technical field [0001] The invention relates to the field of building material detection, in particular to a method and method for preparing a microscopic analysis sample of a double-layer asphalt diffusion system. Background technique [0002] In recent years, with the development of my country's highways, the road network has gradually improved, and a large number of asphalt pavements have greatly shortened their service life due to the problem of overloading and overloading. Due to the environmental benefits, economic benefits and use value produced by waste asphalt pavement (RAP), many scholars began to study the recycling of waste asphalt mixture, and the research and application of recycled asphalt mixture came into being. When recycling waste asphalt mixture, the diffusion of new asphalt in old asphalt cannot be ignored, and the real state of diffusion of new asphalt in old asphalt and the degree of mixing of the two directly affect the actual project. Performance of...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N1/28
CPCG01N1/28
Inventor 崔亚楠李雪杉张淑艳崔树宇
Owner INNER MONGOLIA UNIV OF TECH
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