Perforated capsules
A technology of capsules and hard capsules, applied in microcapsules, capsule transportation, packaged food, etc., can solve the problems of slowing down the dissolution rate of cross-linking trend, unstable chemical angle, unstable microorganisms, etc.
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Embodiment 1
[0057] Embodiment 1: Preparation of microbeads containing menthol
[0058] Part A: Preparation of Bead Coating Layer
[0059] 1. Prepare the outer coating layer using the ingredients in Table 1. Purified water was heated to 30 °C.
[0060] 2. Add glycerin, isomalt and mix.
[0061] 3. The gelatin was then added and the solution was brought to 60°C and mixed for at least one hour until dissolved.
[0062] Part B: Preparation of fill solution and formation of capsules
[0063] 1. Vegetable oil melts at about 40-55°C.
[0064] 2. Then add menthol until dissolved.
[0065] 3. Then add the silica while mixing and homogenize for about 20 minutes while mixing at about 30°C to 45°C.
[0066] 4. The material is extruded through a double nozzle and falls into a cooling solution containing vegetable oil.
[0067] 5. Collect the capsules and drain the remaining oil.
[0068] Table 1
[0069] Material mg / capsule % weight / weight Batch weight (g) coating...
Embodiment 2
[0070] Example 2: Preparation of filled capsules comprising microbeads
[0071] Three microbeads prepared in Example 1 were added to perforated gelatin capsules. Place the beads in a size zero capsule.
[0072] Perforations were made with a DPSS laser - SAML-03-N0500 (3 Watt) manually with variable timing as the capsule was rotated on the mandrel to orientate the laser.
[0073] Holes were drilled using 0.5 mm and 1.0 mm hole diameters with 4 rows of 3 or 4 holes evenly spaced across the diameter of the capsule body and a single hole at the crown of the capsule body.
Embodiment 3
[0074] Example 3: Filling material using compressed granules (briquettes)
[0075] Compressed granules are prepared for inclusion in perforated capsules. Materials are described in Table 2.
[0076] Table 2: Materials used for compressed granules
[0077]
[0078]
[0079] a: Commercially available from Mallicrodt Corporation under the tradename Compap
[0080] b: Commercially available from Ashland Corporation under the tradename Plasdone S 630
[0081] c: Commercially available from FMC Corporation under the tradename Avicel PH101
[0082] Blending and Compression Procedures:
[0083] 1. Sieve all ingredients through a #20 mesh stainless steel sieve
[0084] 2. Blend all ingredients in a turbo mixer for 5 minutes
[0085] 3. A 1.5 g tablet mass was made at 5000 lbs of compression force using a 11 / 16 flat beveled (FFBE) tool
[0086] 4. The tablet mass is then ground into large granules using a mortar and pestle
[0087] 5. Sieve the resulting large granules...
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