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Hot-pressing sintering process for improving density of ceramic material

A hot-pressing sintering and ceramic material technology, applied in the field of ceramic manufacturing, can solve the problems of low efficiency, low efficiency, and the shape change of ceramic parts, and achieve the effects of improving smoothness and uniformity, increasing specific surface area, and high production efficiency

Active Publication Date: 2020-11-17
赛福纳米科技(徐州)有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in this method, it is difficult to cut and crush high-strength graphite, and the efficiency is low, and the uniformity of powder thickness after high-strength graphite powder is added to the graphite sleeve mold is poor, which easily causes changes in the shape of ceramic parts, and is not suitable for the manufacture of bulletproof ceramic plates.
In addition, this method can only sinter one ceramic piece at a time, and the efficiency is not high

Method used

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  • Hot-pressing sintering process for improving density of ceramic material
  • Hot-pressing sintering process for improving density of ceramic material
  • Hot-pressing sintering process for improving density of ceramic material

Examples

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Embodiment 1

[0025] This embodiment relates to a hot pressing sintering process for increasing the density of bulletproof ceramic materials.

[0026] The green body is prepared before hot pressing and sintering, including the following processes:

[0027] 20kg of B 4 C powder (Saifu Nanotechnology), 2kg of nano-carbon fiber (Suzhou First Element CNTcr), 580g of water-soluble phenolic resin and 23kg of high-purity water are evenly mixed to obtain a ceramic slurry; then spray-dried, spray-dried air inlet temperature at 200°C, and the air outlet temperature at 100°C, the composite raw meal is obtained; finally, it is cold-pressed under a pressure of 350MPa into such figure 1 Shown, a ceramic green body 6 with a thickness of 20 mm.

[0028] The hot pressing sintering process includes the following steps:

[0029] S1, using a graphite sleeve mold 1 whose inner cavity matches the shape of the ceramic green body, put the corresponding high-strength graphite lower briquetting block 2 into the b...

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Abstract

The invention discloses a hot-pressing sintering process for improving density of a ceramic material and belongs to the technical field of ceramic manufacturing. The hot pressed sintering process comprises the following steps: S1, putting a high-strength graphite pressing block into a graphite sleeve mold, and fixing the position of the pressing block at the bottom of the mold; S2, sequentially laminating the carbon fiber cloth and the ceramic green body which are consistent in section shape and size into a graphite sleeve mold above a lower pressing block according to the sequence of the carbon fiber cloth, the ceramic green body and the carbon fiber cloth, and placing the laminated fabrics above a lower pressing block in thegraphite sleeve mold; S3, under the pressure of 30-60 MPa, heating the mold 2000-2400 DEG C, and carrying out heat preservation and pressure maintaining gor 10-60 min, wherein a high-strength graphite upper pressing head is pressed downwards to pressurize the ceramic material, and finally the ceramic green body is subjected to hot pressing sintering to form the bulletproof ceramic plate. By using the carbon fiber cloth, the smoothness and uniformity of exhausting gas in the ceramic material powder during hot pressing sintering are improved, and the composite armor based on the bulletproof ceramic plate is suitable for manufacturing the bulletproof ceramicplate and can enhance the capability of resisting multiple strikes of armor-piercing bombs and armor-piercing incendiary bombs of the composite armor based on the bulletproof ceramic plate.

Description

technical field [0001] The invention relates to a technology in the field of ceramic manufacturing, in particular to a hot-pressing sintering process for increasing the density of ceramic materials. Background technique [0002] Hot pressing sintering is a commonly used process in the manufacture of ceramic materials. Since the longitudinal pressure is applied to supplement the sintering driving force, the densification of ceramics can be achieved in a short sintering time, and a relatively dense bulk ceramic material can be obtained. Especially for ceramic materials containing covalent bonds that are difficult to sinter, such as B 4 C, SiC, Si 3 N 4 , the advantages of this process are obvious. [0003] For the mold material for hot pressing sintering, whether it is the large outer mold or the upper and lower compacts, high-strength graphite materials with ultra-fine particle structure, high purity and high degree of graphitization are used, which have a dense structure ...

Claims

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Application Information

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IPC IPC(8): C04B35/80C04B35/563C04B35/645
CPCC04B35/645C04B35/563C04B2235/5248C04B2235/602C04B2235/656C04B2235/6567C04B2235/77C04B2235/96
Inventor 薛平陈玉华董明
Owner 赛福纳米科技(徐州)有限公司
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