Microwave self-repairable polypropylene-carbon-based composite material and preparation method thereof
A technology of carbon-based composite materials and carbon-based materials, applied in the field of polypropylene-carbon-based composite materials and their preparation, to achieve good self-healing effects, improve dispersion and compatibility
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Embodiment 1
[0097] A microwave self-healing polypropylene-carbon-based composite material is prepared from the following components by weight:
[0098]
[0099] The preparation method of self-healing polypropylene masterbatch is as follows:
[0100]1) Mix 2000-mesh carbon black and phenyltrimethoxysilane in a mixer at a mass ratio of 5:1, the speed of the mixer is 200r / min, and the mixing time is 2min;
[0101] 2) Continue to add polypropylene powder to the mixer, the mass ratio is 1:2 according to the total mass of the material in step 1) and the polypropylene powder (the particle size is 0.1mm, the melt index is 20g / 10min), and then Continue to mix with a mixer, the speed of the mixer is 200r / min, and the mixing time is 2min;
[0102] 3) The mixed material in step 2) is fed into the twin-screw extruder through the main feeder, then melted and extruded, and granulated to obtain self-repairing polypropylene masterbatch.
[0103] The process parameters of the twin-screw extruder are a...
Embodiment 2
[0108] A microwave self-healing polypropylene-carbon-based composite material is prepared from the following components by weight:
[0109]
[0110] The preparation method of self-healing polypropylene masterbatch is as follows:
[0111] 1) Mix 2000-mesh carbon black and phenyltrimethoxysilane in a mixer at a mass ratio of 5:1, the speed of the mixer is 200r / min, and the mixing time is 2min;
[0112] 2) Continue to add polypropylene powder to the mixer, the mass ratio is 1:2 according to the total mass of the material in step 1) and the polypropylene powder (the particle size is 0.1mm, the melt index is 20g / 10min), and then Continue to mix with a mixer, the speed of the mixer is 200r / min, and the mixing time is 2min;
[0113] 3) The mixed material in step 2) is fed into the twin-screw extruder through the main feeder, then melted and extruded, and granulated to obtain self-repairing polypropylene masterbatch.
[0114] The process parameters of the twin-screw extruder are ...
Embodiment 3
[0119] A microwave self-healing polypropylene-carbon-based composite material is prepared from the following components by weight:
[0120]
[0121] The preparation method of self-healing polypropylene masterbatch is as follows:
[0122] 1) Mix 2000-mesh carbon black and phenyltrimethoxysilane in a mixer at a mass ratio of 5:1, the speed of the mixer is 200r / min, and the mixing time is 2min;
[0123] 2) Continue to add polypropylene powder to the mixer, the mass ratio is 1:2 according to the total mass of the material in step 1) and the polypropylene powder (the particle size is 0.1mm, the melt index is 20g / 10min), and then Continue to mix with a mixer, the speed of the mixer is 200r / min, and the mixing time is 2min;
[0124] 3) The mixed material in step 2) is fed into the twin-screw extruder through the main feeder, then melted and extruded, and granulated to obtain self-repairing polypropylene masterbatch.
[0125] The process parameters of the twin-screw extruder are ...
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