Antibacterial film product and preparation process
A technology of thin film products and preparation process, which is applied in the field of plastic products, can solve the problems of affecting the long-lasting antibacterial effect, the antibacterial durability needs to be improved, and the ultra-fine antibacterial agent powder, so as to increase stability and weather resistance and prevent growth. With agglomeration, long-lasting antibacterial effect
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preparation example 1
[0054] The preparation method of silicate / silver composite powder comprises the following steps:
[0055] 1) Set the molar concentration to 0.5×10 -3 mol / L silver nitrate solution and polyvinylpyrrolidone aqueous solution with a mass concentration of 1.2% are mixed in a volume ratio of 4:1 to obtain a mixed solution;
[0056] 2) Mix 80 g of the mixed solution in step 1) with 3 g of kaolin to obtain a reaction solution, and stir for 4 hours;
[0057] 3) After adding 0.2 g of glucose to the reaction solution to continue the reaction for 2 hours, filter and dry at 60° C. for 24 hours to obtain a silicate / silver composite powder;
[0058] Among them, the average particle size of kaolin is 20-30 μm.
preparation example 2
[0060] The preparation method of silicate / silver composite powder comprises the following steps:
[0061] 1) Set the molar concentration to 1.5×10 -3 mol / L silver nitrate solution and polyvinylpyrrolidone aqueous solution with a mass concentration of 1% are mixed in a volume ratio of 4.5:1 to obtain a mixed solution;
[0062] 2) Mix 90 g of the mixed solution in step 1) with 2.5 g of kaolin to obtain a reaction solution, and stir for 4.5 hours;
[0063] 3) After adding 0.3 g of glucose to the reaction solution to continue the reaction for 1.5 h, filter and dry at 60° C. for 24 h to obtain a silicate / silver composite powder;
[0064] Among them, the average particle size of kaolin is 20-30 μm.
preparation example 3
[0066] The preparation method of silicate / silver composite powder comprises the following steps:
[0067] 1) Set the molar concentration to 2×10 -3 mol / L silver nitrate solution and polyvinylpyrrolidone aqueous solution with a mass concentration of 0.8% are mixed in a volume ratio of 5:1 to obtain a mixed solution;
[0068] 2) Mix 100 g of the mixed solution in step 1) with 2 g of kaolin to obtain a reaction solution, and stir for 5 hours;
[0069] 3) After adding 0.5 g of glucose to the reaction solution to continue the reaction for 1 hour, filter and dry at 60° C. for 24 hours to obtain a silicate / silver composite powder;
[0070] Among them, the average particle size of kaolin is 20-30 μm.
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