Hepatitis B virus rapid detection system combining MCDA with biosensor
A biosensor, hepatitis B virus technology, applied in the determination/inspection of microorganisms, methods based on microorganisms, microorganisms, etc., can solve the problems of low detection sensitivity, high cost of detection methods, and long time consumption.
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Embodiment 1
[0053] 1. Materials and Equipment
[0054] Genomic DNA and RNA extraction kits were purchased from Xi’an Tianlong Technology, the colorimetric indicator (Colorimetric indicator) was purchased from Malachite Green Company, the universal constant temperature amplification kit was purchased from Beijing Haitai Zhengyuan, and biotin-labeled BSA (bovine serum albumin) Purchased from Abcam Corporation. LFB materials include backsheets, sample pads, absorbent pads, conjugate pads, and NC membranes, all of which were purchased from Jie-Yi Biotechnology.Co.Ltd. Nanoparticle-coupled streptavidin (dark red, Dye streptavidin-coated polymer nanoparticles) was purchased from Bangs Laboratories. HBV real-time PCR detection kit was purchased from DaAn Gene Company. Nucleic acid purity and concentration were analyzed by Nano-Drop ND-2000 (A260 / 280).
[0055] 2. MCDA primer design
[0056] Design primers according to the S gene of hepatitis B virus (the sequence of the S gene is shown in Ge...
Embodiment 2
[0065] Embodiment 2: MCDA optimal reaction temperature test
[0066] In this embodiment, it is basically the same as in Example 1, except that the difference lies in the setting of temperature. In this experimental example, the optimum reaction temperature of MCDA is detected and confirmed, and the amplification temperature is set at 60-67° C. (every 1° C. is a gradient). Use a real-time turbidimeter (LA-500) to detect amplicons in the system (turbidity greater than 0.1 is considered a positive result). Experimental results such as image 3 and Figure 4 As shown (the turbidity detector uses the judgment mode to mainly examine the amplification time), 63°C is the optimal reaction time.
Embodiment 3
[0067] Embodiment 3: the sensitivity test of MCDA-LFB
[0068] Dilute the HBV template to a nucleic acid content of 5.0 × 10 3 IU, 5.0×10 2 IU, 5.0×10 1 IU, 5IU, 5IU, 0.5IU, 0.05IU, obtain 7 kinds of diluted templates, then carry out MCDA amplification (same as Example 1) with the above templates respectively, and carry out colorimetric indicator detection and LFB detection to MCDA amplification products . Experimental results such as Figure 5 As shown, the detection sensitivity of this scheme is that the amount of HBV in each reaction is 5 IU (ie LoD, limited of detection).
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