Composition for relieving cough and reducing sputum and preparation method thereof
A technology for relieving cough and removing phlegm and a composition is applied in the field of the composition for relieving cough and removing phlegm and its preparation, and can solve the problems of poor patient experience, disappearance and high temperature
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[0066] Preparation of reference solution: Take an appropriate amount of psoralen reference substance, accurately weigh it, put it in a 50mL volumetric flask, add an appropriate amount of methanol, and ultrasonically (power 100W, frequency 40kHz) to dissolve (water temperature rises about 1°C) , cooled to room temperature, added methanol to the mark, shaken well, and prepared a solution with a concentration of psoralen of 0.188 mg / mL.
[0067] Preparation of the test solution: take 0.5g of the test sample, accurately weigh it, place it in a 50mL conical flask with a stopper, accurately add 30mL of 50% methanol solution, extract by ultrasonic (power 100W, frequency 40kHz) for 30min, filter, The solvent was recovered from the filtrate to dryness, the residue was dissolved in methanol, transferred to a 5mL volumetric flask, diluted to the mark with methanol, shaken up, filtered through a 0.22 μm microporous membrane, and the subsequent filtrate was taken as the test solution.
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Embodiment 1
[0089] Example 1 A kind of composition with the effect of relieving cough and resolving phlegm
[0090] The composition described in this embodiment is made of the following traditional Chinese medicine composition as raw material:
[0091] 20 parts by weight of five-finger peach, 5 parts by weight of Polygonatum japonica, 2 parts by weight of mulberry leaves and 2 parts by weight of Luo Han Guo; wherein 1 part by weight = 1 kg.
[0092] According to the optimized process of Research Example 1, continuous extraction and concentration were carried out in a continuous extraction and separation concentrator, and the concentrated solution was spray-dried (inlet air temperature 160°C, outlet air temperature 60°C) to obtain.
Embodiment 2
[0093] Example 2 A kind of composition with the effect of relieving cough and resolving phlegm
[0094] The composition described in this example is made of the following traditional Chinese medicine composition as a raw material:
[0095] 30 parts by weight of five-finger peach, 10 parts by weight of Polygonatum japonica, 5 parts by weight of mulberry leaves and 5 parts by weight of Luo Han Guo; wherein 1 part by weight = 1 kg.
[0096] According to the optimized process of Research Example 1, continuous extraction and concentration were carried out in a continuous extraction and separation concentrator, and the concentrated solution was spray-dried (inlet air temperature 165°C, outlet air temperature 65°C) to obtain.
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