Composition with sedative and sleep-aiding effects and application thereof
A technology of composition and efficacy, applied in the field of medicine, can solve problems such as poor and adverse reaction effects, and achieve the effect of high safety
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[0042] 2.1.1 Preparation of test liquid:
[0043] Preparation of blank milk: Weigh 25g of glycerin and dissolve it in 500ml of water for injection, weigh 12g of soybean lecithin and disperse it in the glycerin solution, and place it in a high-shear emulsifier to disperse evenly until a stable fat emulsion submicroemulsion solution is formed. Filter through a microporous membrane, aliquot, spin sterilize, and use as blank milk.
[0044]Preparation of CBD sub-microemulsion: Weigh 25g of glycerin and dissolve it in 500ml of water for injection, weigh 12g of soybean lecithin and disperse it in the glycerin solution, and place it in a high-shear emulsifier to disperse evenly; accurately weigh 0.0943g of CBD crystals and dissolve it in 100g In coconut oil, add 2g of oleic acid and mix well to obtain a CBD oil solution; add the CBD oil solution into a high-shear emulsifier at a constant speed to prepare a fat emulsion solution, and add water for injection to 1000ml until a stable fat...
Embodiment 1-3 and comparative example 1-4
[0066] Weigh 250g of glycerin and dissolve it in 5000ml of water for injection, weigh 120g of soybean lecithin and disperse it in the glycerin solution, and place it in a high-shear emulsifier to disperse evenly; accurately weigh 0.2563g of CBD crystals, 0.0431g of THC crystals, and 0.0864g of CBN crystals Dissolve in 1000g (400g of sweet almond oil, 300g of coconut oil, 300g of linseed oil) mixed oil, add 20g of oleic acid and mix to obtain an oil phase; add the oil phase into a high-shear emulsifier at a uniform speed to prepare a fat emulsion solution , add water for injection to 10000ml, until a stable fat emulsion submicroemulsion solution is formed, filter through a microporous membrane, subpackage, and spin sterilize, as the test drug solution of Example 2, the content of CBD is 0.02559mg / ml, THC Content of 0.00428mg / ml, CBN content of 0.00856mg / ml (ratio about 6:1:2); according to this method to prepare other examples and comparative examples for testing liquid.
[006...
Embodiment 4-6 and comparative example 5-8
[0112] Weigh 250g of glycerin and dissolve it in 5000ml of water for injection, weigh 120g of soybean lecithin and disperse it in the glycerin solution, and place it in a high-shear emulsifier to disperse evenly; accurately weigh 0.2563g of CBD crystals, 0.0431g of THC crystals, and 0.0864g of CBN crystals Dissolve in 1000g (400g of sweet almond oil, 300g of coconut oil, 300g of linseed oil) mixed oil, add 20g of oleic acid and mix to obtain an oil phase; add the oil phase into a high-shear emulsifier at a uniform speed to prepare a fat emulsion solution , add water for injection to 10000ml, until a stable fat emulsion submicroemulsion solution is formed, filter through a microporous membrane, subpackage, and spin sterilize, as the test drug solution of Example 2, the content of CBD is 0.02559mg / ml, THC Content of 0.00428mg / ml, CBN content of 0.00856mg / ml (ratio about 6:1:2); according to this method to prepare other examples and comparative examples for testing liquid.
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