All-solid-state secondary battery
A secondary battery and all-solid technology, applied in the direction of secondary batteries, solid electrolytes, battery electrodes, etc., can solve the problems of small capacity, high manufacturing cost, thick active material layer or high layering difficulty, and achieve the best heat dissipation The effect of high uniformity
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Embodiment 1~6
[0123] (Production of Cu particles with an oxide film)
[0124] As for the Cu particles with an oxide film in Examples 1 to 6, in N 2 Cu particles with a diameter of 1 μm were oxidized at a heat treatment temperature of 200° C. in an atmosphere. As mentioned above, using the XPS device (manufactured by ULVAC-PHI, PHI Quantera II), it is confirmed that there is an oxide film on the surface of the particle after the treatment, and the conditions are adjusted until the desired film thickness is obtained, and an oxide film with a thickness of 0.01 μm is produced. of metal particles.
[0125] (Preparation of Paste for Outermost Solid Electrolyte Layer)
[0126] As far as the production of the outermost solid electrolyte layer paste is concerned, Li 1+x Al x Ti 2-x (PO 4 ) 3 (0≤x≤0.6) and Cu particles having an oxide film were mixed in a predetermined weight ratio, and 100 parts of ethanol and 200 parts of toluene were added to 100 parts of the powder as a solvent, and wet mi...
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