Fluorescent PCR primer group for specifically recognizing IYVLVMLVL peptide fragment and application thereof
A primer set and specific technology, applied in the field of genetic engineering, can solve problems such as undiscovered
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Embodiment 1
[0025] Example 1 primer design
[0026] The TCR primers were designed in accordance with the HLAA24 classification, EBV viral antigen peptide IYVLVMLVL L24-2 and L24-49 sites. The sequences of the obtained primers are shown in SEQ ID NO.1 to 4.
Embodiment 2
[0027] Example 2 Standard Curve Establishment
[0028] Taking the L24-2 site of TCR as an example design.
[0029] Take 1 L24-2 site of plasmid DNA standard 10 8 Copy number diluent, 10 7 Copy number diluent, 10 6 Copy number diluent, 10 5 Copy number diluent, 10 4 Copy number diluent, 10 3 Copy number diluent, 10 2 Copy number diluent, 10 1 A copy number diluent is provided in real time fluorescent PCR according to the following reaction system and reaction procedure.
[0030] Reaction system: PCR premix 10 μL; positive primer 0.4 μL, primer concentration: 10 μm / μl; reverse primer: 10 μm / μl; ROX Reference Dye (50 ×) 0.2 μL; TCR-T cell medicine Genomic DNA2 μL, concentration 50 ng / μL, or TCR plasmid standard DNA2 μL; Nuclease-Free Water 7 μL; total reaction system is 20 μL.
[0031] PCR react procedures: 95 ° C, 30S; (95 ° C, 5S; 60 ° C, 20S) 40 cycles. Set the reference fluorescence to ROX, select the type of reaction to Sybr Green Reagents, select the fluorescence detectio...
Embodiment 3
[0036] Example 3 Sensitivity detection
[0037] The genomic DNA stock, 10-fold dilution, 100-fold dilution, 1000-fold dilution, 10000-fold dilution, 1000-fold dilution, 10000 times dilution, 1000-fold dilution, 10000 times dilution, 1000-fold dilution, 10000 times dilution, reaction system and procedure of real-time fluorescent PCR according to Example 2 Making amplification. Amplification curve of genomic DNA for TCR-T cell medicines for L24-2 sites Figure 4 Indicated. The amplified product is subjected to agarose gel electrophoresis. Figure 5 Indicated.
[0038] The CT value of the genomic DNA of each dilution of the TCR-T cell medicine was produced into the standard curve of Embodiment 2, and the copy number of the genomic DNA of the TCR-T cell medicine of each dilution can be calculated.
[0039] After calculation, the copy number of the TCR-T cell medicine genome DNA stock solution for the L24-2 site is 46,766 copies, and the number of copies of the 10-fold dilution is 7998 c...
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