Waterproof locking agent and preparation method thereof
A technology of waterproof locking agent and active agent, applied in chemical instruments and methods, drilling composition and other directions, can solve the problems of reduced oil and gas permeability, reduced oil and gas recovery rate, etc., to reduce oil-water interfacial tension and reduce surface tension. , the preparation method is simple
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Embodiment 1
[0025] Weigh 5g XP30, 10g sodium lauryl sulfate, 6g cocamidopropyl betaine and 74g water into a beaker, stir on a magnetic stirrer at 200rpm for 0.5h to make the system evenly stirred, then slowly drop into the beaker Add 5g of n-butanol, after the dropwise addition is complete, keep the stirring speed of the magnetic stirrer at 200rpm, and stir for 0.5h to obtain a clear and transparent waterproof locking agent. Make a 0.1% solution to measure the contact angle with a contact angle meter, and measure the surface tension and interfacial tension with an interfacial tensiometer.
Embodiment 2
[0027] Weigh 10g XP30, 15g sodium lauryl sulfate, 8g cocamidopropyl betaine and 62g water into a beaker and stir on a magnetic stirrer at 200rpm for 1h to make the system evenly stirred, then slowly drop into the beaker 5g of n-butanol, after the dropwise addition is complete, keep the stirring speed of the magnetic stirrer at 200rpm, and stir for 0.5h to obtain a clear and transparent waterproof locking agent. Make a 0.1% solution to measure the contact angle with a contact angle meter, and measure the surface tension and interfacial tension with an interfacial tensiometer.
Embodiment 3
[0029] Weigh 5g XP40, 10g sodium dodecyl sulfonate, 5g cocamidopropyl betaine and 75g water into a beaker, stir on a magnetic stirrer at 200rpm for 1h min to make the system evenly stirred, then slowly pour into the beaker Add 5g of n-butanol dropwise. After the dropwise addition is complete, keep the stirring speed of the magnetic stirrer at 200rpm and stir for 1 hour to obtain a clear and transparent waterproof locking agent. Make a 0.1% solution to measure the contact angle with a contact angle meter, and measure the surface tension and interfacial tension with an interfacial tensiometer.
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