Graphene oxide and titanium dioxide composite photocatalyst, cleaning mask and preparation method of cleaning mask
A technology of titanium dioxide and graphene, applied in the direction of physical/chemical process catalysts, chemical instruments and methods, cosmetic preparations, etc., can solve problems such as easy leakage, easy skin irritation, peeling, etc., and achieve easy portability, prevention of acne, Strong cleaning effect
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[0058]According to a method for preparing a graphene oxide-titanium dioxide composite photocatalyst provided in an embodiment of the second aspect of the present invention, preparing the graphene oxide-titanium dioxide composite photocatalyst described in the graphene oxide photocatalytic cleaning mask includes the following steps:
[0059] Step 1: mixing deionized water and absolute ethanol to obtain a mixed solution 1; dispersing graphene oxide into the mixed solution 1, and ultrasonically dissolving it uniformly to obtain a graphene oxide solution;
[0060] Step 2: adding the titanium-containing substance into the graphene oxide solution and stirring, after stirring evenly, adding acid and deionized water in turn, and continuing to stir until uniform, to prepare a precursor solution containing titanium element and graphene oxide;
[0061] Step 3: Pour the precursor solution into the reaction kettle, keep the first predetermined temperature for the first predetermined time, c...
Embodiment 1
[0077] Such as figure 1 As shown, the flow chart of preparing graphene oxide photocatalytic cleansing mask with titanium dioxide as titanium source in the embodiment of the present invention. Specific steps are as follows:
[0078] Step 1 S01: Mix deionized water and absolute ethanol at a volume ratio of 2:1, weigh a certain amount of graphene oxide, disperse it into the above solution, and dissolve it ultrasonically for 2 to 3 hours to prepare graphite oxide Alkene solution.
[0079] Step 2 S02: Add a certain amount of titanium dioxide to the graphene oxide solution, stir magnetically for 1 to 2 hours, and then ultrasonically clean for 30 minutes to prepare a precursor solution containing titanium and graphene oxide.
[0080] Step 3 S03: Pour the precursor solution into the reaction kettle, maintain the first predetermined temperature for the first predetermined time, cool the container after the reaction, remove the supernatant, perform centrifugation, wash the precipitate...
Embodiment 2
[0093] Such as figure 2 As shown, in the embodiment of the present invention, using tetrabutyl titanate as a titanium source to prepare a flow chart of graphene oxide photocatalytic cleaning mask, the specific steps are as follows:
[0094] Step 1 S01: Take deionized water and absolute ethanol and mix according to the volume ratio of 2:1, weigh a certain amount of graphene oxide, disperse it into the above solution, and ultrasonically dissolve it for 2 hours to 3 hours to prepare Obtain graphene oxide solution.
[0095] Step 2 S02: Take a certain amount of tetrabutyl titanate and add it to the above graphene oxide solution, stir magnetically for 1 hour to 2 hours until it is transparent and uniform, and then add a certain amount of acetic acid and deionized water dropwise to continue Stir for one hour to two hours to prepare a precursor solution containing titanium element and graphene oxide.
[0096] Step 3 S03: Pour the precursor solution into the reaction kettle, maintai...
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