Plug-shaped implant for the replacement and regeneration of biological tissue and method for preparing the implant
A technology of biological tissue and implants, applied in the field of implants, can solve problems such as degeneration, cartilage tissue unable to withstand joint biomechanical challenges, and delay
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example 1
[0086] Example 1: Polycarbonate-aliphatic: Poly(hexamethylene carbonate urethane)-diurea biomaterial MVH313, see Table 1 below.
[0087] This one-pot two-step biomaterial MVH313 was prepared by using 2.0 molar equivalents of 1,6-diisocyanatohexane to 1.0 molar equivalents of poly(hexamethylene carbonate) diol (MW=2000) Functionalization (step 1) and subsequent chain extension (step 2) were performed using 1.0 molar equivalent of 1,6-diaminohexane.
[0088] Specifically, the aliphatic poly-urethane-urea-hexamethylene carbonate biomaterials of the middle section 3 and the top section 4 were produced as follows (ref. image 3 ). Poly(hexamethylene carbonate) diol (MW=2000; 23.9 g, 11.9 mmol) was weighed in a 500 mL 3-neck flask and dried under vacuum by heating to 75° C. overnight and then allowed to cool to room temperature. Under argon atmosphere, 1,6-diisocyanatohexane (4.1 g, 23.9 mmol), DMAc (20 mL) and a drop of Sn(II) bis(2-ethylhexanoate) were added after which the mi...
example 2
[0092] Example 2 : polyether-aromatic: poly(tetrahydrofurancarbamate)-diurea biomaterial MVH309B, see Table 1 below.
[0093] Biomaterial MVH309B was also produced in a one-pot two-step experimental procedure similar to that described in detail for biomaterial MVH313. Specifically, biomaterial MVH309B was prepared by functionalizing 1.0 molar equivalents of poly-tetrahydrofuran diol (MW=2000) with 1.33 molar equivalents of bis(4-isocyanatophenyl)methane (MDI) (step 1), and then chain extension (step 2) using 0.33 molar equivalents of 1,6-diaminohexane. Biomaterial MVH309B was isolated as a white, flexible, tough elastomeric polymer.
example 3
[0094] Example 3: Polyether-aliphatic: Poly(tetrahydrofurancarbamate)-diurea biomaterial MVH312, see Table 1 below.
[0095] Biomaterial MVH312 was also produced in a one-pot two-step experimental procedure similar to that described in detail for biomaterial MVH313. Specifically, biomaterial MVH312 was prepared by functionalizing 1.0 molar equivalents of poly-tetrahydrofuran diol (MW=2000) with 2.0 molar equivalents of 1,6-diisocyanatohexane (step 1) , and followed by chain extension using 1.0 molar equivalent of 1,6-diaminohexane (step 2). The biomaterial MVH312 was isolated as a flexible, tough elastomeric polymer.
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