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Lithium disilicate glass ceramic restoration and preparation method thereof

A lithium disilicate and glass ceramic technology, which is applied in dental preparations, dental prostheses, pharmaceutical formulations, etc., can solve problems such as complex preparation processes, achieve good aesthetic effects, save raw material costs, and improve the effect of powder utilization.

Pending Publication Date: 2022-02-11
SHENZHEN UPCERA DENTAL TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, the main disadvantage of the sintering method is that the preparation process is relatively complicated.

Method used

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  • Lithium disilicate glass ceramic restoration and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0079]

[0080] The intraoral scanner is used to scan and obtain the three-dimensional shape data of the tooth to be restored and the adjacent teeth, and the obtained three-dimensional shape data is directly imported into the CAD software, and the crown shape is designed on the CAD software platform, and the obtained crown shape data is imported into the 3D printer;

[0081] According to the formula 1 in Table 1, the components are selected, mixed evenly, put into a platinum crucible and melted at a high temperature in a muffle furnace, the melting temperature is 1250 ° C; the molten glass liquid is water quenched to form a lithium disilicate glass frit, and the obtained two Lithium silicate glass frit is pulverized by airflow to obtain particle size D 50 Lithium disilicate glass-ceramic powder of 10 μm;

[0082] The obtained particle size D 50 Lithium disilicate glass-ceramic powder with a thickness of 10 μm was put into the hopper of a 3D printer, and the 3D printer was u...

Embodiment 2

[0087]

[0088] The intraoral scanner is used to scan and obtain the three-dimensional shape data of the tooth to be restored and the adjacent teeth, and the obtained three-dimensional shape data is directly imported into the CAD software, and the crown shape is designed on the CAD software platform, and the obtained crown shape data is imported into the 3D printer;

[0089] According to the formula 2 in Table 1, the components were selected, mixed evenly, put into a platinum crucible and melted at a high temperature in a muffle furnace at a melting temperature of 1650°C; the molten glass liquid was water-quenched to form a lithium disilicate glass frit, and the resulting two Lithium silicate glass frit is crushed by air flow to obtain particle size D 50 Lithium disilicate glass-ceramic powder of 20 μm;

[0090] After comparing the tooth to be restored and the adjacent tooth with the color guide, obtain the color information, and select the colorant and fluorescent agent sho...

Embodiment 3

[0096]

[0097] Use a 3D scanner to scan to obtain the 3D shape data of the tooth to be restored and the adjacent teeth, and the obtained 3D shape data are directly imported into the CAD software, and the crown shape is designed on the CAD software platform, and the data of the crown shape is imported into the 3D printer;

[0098] According to the formula 3 in Table 1, the components were selected, mixed evenly, put into a platinum crucible and melted at a high temperature in a muffle furnace, the melting temperature was 1450°C; the molten glass liquid was water-quenched to form a lithium disilicate glass frit, and the obtained two Lithium silicate glass frit is crushed by air flow to obtain particle size D 50 Lithium disilicate glass-ceramic powder of 15 μm;

[0099] After comparing the tooth to be restored and the adjacent tooth with the shade guide, obtain color information, and select the colorant and fluorescent agent as shown in 2-3 in Table 2 according to the obtained...

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Abstract

The invention provides a lithium disilicate glass ceramic restoration and a preparation method thereof. The method for preparing the lithium disilicate glass ceramic restoration by the selective laser sintering molding technology comprises the step of carrying out selective laser sintering molding on lithium disilicate glass ceramic powder or powder containing pigments and fluorescent agents by utilizing a 3D printer to obtain the lithium disilicate glass ceramic restoration. According to the preparation method provided by the invention, the powder utilization rate is increased, the raw material cost is saved, forming before sintering is not needed, the light transmittance and / or color gradient of the obtained lithium disilicate glass ceramic restoration can be realized, and a better aesthetic effect is achieved.

Description

technical field [0001] The invention relates to the technical field of glass ceramics, in particular to a lithium disilicate glass ceramic restoration and a preparation method thereof. Background technique [0002] Li 2 O-SiO 2 In the binary glass system, Li 2 Si 2 o 5 Lithium disilicate (Li 2 O 2SiO 2 ) Glass-ceramic polycrystalline materials are well known. Due to its high mechanical strength, good machinability and semipermeability, lithium disilicate glass ceramics are widely used in dental restorations, articular fossa replacement materials, tableware, and disk substrates. [0003] Dental lithium disilicate glass-ceramic restorations are mainly produced by casting. In the production process of the casting method, since the colorant and fluorescent agent are melted together with the glass ceramic ingredients at high temperature, its color stability is difficult to control. At the same time, the degree of automation of the casting process is low and the productio...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K6/833A61K6/78A61K6/70C03C10/04B33Y70/00
CPCA61K6/833A61K6/78A61K6/70C03C10/00B33Y70/00
Inventor 韩成玮陈拥庆宋国轶王彦宇刘颖
Owner SHENZHEN UPCERA DENTAL TECH