Corrosion-resistant coating for photovoltaic power station box and preparation method thereof
A photovoltaic power station, corrosion-resistant technology, applied in the field of coatings, can solve the problems of reducing the adhesion between coatings and metal substrates, damage to metal substrates, etc., achieve excellent adhesion, fast curing speed, and improve corrosion resistance.
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Embodiment 1
[0021] Preparation of Epoxidized Branched Fluorides:
[0022] Step A, add 120 mL of acetic acid to the four-necked flask with condensation device, thermometer and stirring device, then add 0.011 mol [3-(trimethoxysilyl) propyl] succinic anhydride, be warming up to reflux, and in a stirring state 0.01 mol of 4-aminobutyric acid was added in batches, and after the addition was complete, the reflux reaction was continued for 10 hours, and then the temperature was reduced to 30° C. to remove ethanol by rotary evaporation under reduced pressure to obtain a siloxane-containing dicarboxylic acid;
[0023] Step B: After mixing 0.41 mol of siloxane-containing dicarboxylic acid and 0.1 mol of pentaerythritol, add 4.44 g of p-toluenesulfonic acid, then heat to 70 ° C, stir and react for 4 h, then reduce to 35 ° C for vacuum and rotary evaporation to obtain branch;
[0024] Step C, after mixing 153 g of branched product and 92 g of bisphenol AF uniformly, adding 6.12 g of p-toluenesulfon...
Embodiment 2
[0027] Preparation of Epoxidized Branched Fluorides:
[0028] Step A, add 160mL acetic acid to the four-necked flask with condensation device, thermometer and stirring device, then add 0.013mol [3-(trimethoxysilyl)propyl] succinic anhydride, be warming up to reflux, and in a stirring state 0.01 mol of 4-aminobutyric acid was added in batches, and after the addition was complete, the reflux reaction was continued for 10 hours, and then the temperature was reduced to 30° C. to remove ethanol by rotary evaporation under reduced pressure to obtain a siloxane-containing dicarboxylic acid;
[0029] Step B: After mixing 0.42 mol of siloxane-containing dicarboxylic acid and 0.1 mol of pentaerythritol, add 7.60 g of p-toluenesulfonic acid, then heat to 70° C., stir and react for 4 hours, and then reduce to 35° C. under reduced pressure for rotary evaporation to obtain branch;
[0030] Step C, after mixing 153 g of branched product and 100 g of bisphenol AF uniformly, adding 7.65 g of ...
Embodiment 3
[0033] A corrosion-resistant coating for photovoltaic power station boxes is prepared by the following steps:
[0034] The first step, prepare the following raw materials in parts by weight of component A: 75 parts of epoxidized branched fluorine-containing compound, 15 parts of water-based polyurethane resin; component B is diethylenetriamine, and the mass ratio of component A and component B is is 100: 0.8;
[0035] The second step is to dissolve the water-based polyurethane resin in water and stir evenly, then add the epoxidized branched fluorine-containing compound and stir evenly at room temperature, and finally add diethylenetriamine to obtain a corrosion-resistant coating for photovoltaic power station boxes.
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