Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Phase equilibrium determination and separation device and application method thereof

A separation device and phase balance technology, applied in the field of chemical engineering, can solve the problems of high cost, low applicable temperature, long time required for phase balance, etc., and achieve the effect of good effect and reduced cost

Active Publication Date: 2022-05-03
CHINA PETROLEUM & CHEM CORP +1
View PDF14 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] One of the technical problems to be solved by the present invention is to provide a visually adjustable volume phase balance measurement and separation device suitable for high temperature and high pressure conditions, which overcomes the long time required to achieve phase balance in the prior art, high cost, Insufficient for relatively low temperature

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Phase equilibrium determination and separation device and application method thereof
  • Phase equilibrium determination and separation device and application method thereof
  • Phase equilibrium determination and separation device and application method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0081] Use as attached figure 1 In the phase balance measurement and separation device shown, the balance space in the balance main kettle has an inner diameter of 80mm and a height of 100mm, and the window is a sapphire cylinder with an inner diameter of 10mm and a height of 30mm. The inner diameter of the balance auxiliary kettle is 100mm, and the height is 100mm. The residual oil used was obtained from Wuhan Branch of China Petroleum & Chemical Corporation, and its properties are shown in Table 1.

[0082] Utilize negative pressure to inhale the residual oil 120g after heating in the balance main kettle 8; Utilize the high-precision plunger pump 1 to press the n-butane solvent in the solvent tank 3 into the balance main kettle 8, record the n-butane solvent feed temperature, Pressure and volume: Heat the balanced main kettle 8 to the reaction temperature of 120°C and keep it warm, start stirring, set the 8 pistons of the balanced main kettle to the pressure holding mode of...

Embodiment 2

[0085] The phase balance measurement and separation device, residual oil raw material, and implementation steps used are the same as those in Example 1, except that the stirring time is 4 hours.

Embodiment 3

[0087] The phase balance measurement and separation device, residual oil raw material, and implementation steps adopted are the same as those in Example 1. The difference is that the test solvent is n-pentane, the test temperature is 220° C., and the test pressure is 16 MPa. The obtained phase balance data are listed in the table 2.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
thermal resistanceaaaaaaaaaa
Login to View More

Abstract

The invention discloses a phase equilibrium determination and separation device and an application method thereof. The device comprises a feeding and cleaning system, a main balance kettle, an auxiliary balance kettle and a sampling system which are communicated in sequence, the balance main kettle is composed of an upper balance space and a bottom volume adjusting structure, the balance space is provided with a material inlet, a window is arranged on the wall of the balance space, the top of the balance main kettle is provided with an outlet, and the outlet of the balance main kettle is respectively communicated with the inlets of the balance auxiliary kettle and the sampling system; the auxiliary balance kettle is composed of an upper balance space and a bottom volume adjusting structure, the balance space is provided with an inlet and an outlet, and the outlet of the auxiliary balance kettle is communicated with the inlet of the sampling system. The phase equilibrium determination and separation device provided by the invention adopts a window to observe the movement condition of an interface, the cost of the device is reduced, and the phase equilibrium of a system is not influenced by the separation process of light and heavy phases after extraction.

Description

technical field [0001] The invention belongs to the field of chemical engineering, and relates to a high-temperature, high-pressure, visually adjustable volume phase balance measurement and separation device and a use method thereof. Background technique [0002] Solvent deasphalting technology is one of the important technologies for lightening heavy oil, and its combined process is an attractive development direction for the maximum processing and utilization of heavy oil. Solvent deasphalting is a physical process of liquid-liquid extraction, which is separated according to the different solubility of the solvent to the components in the residue. Although the industrialization of solvent deasphalting process has a long history, due to the extremely complex composition of residual oil, the properties of residual oil from different sources are very different. In order to accurately predict the yield and product properties of deasphalted oil, a reliable basic design is provi...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): B01D11/04C10G21/00C10G21/14C10G21/30G01D21/02
CPCB01D11/0488B01D11/0484B01D11/0492C10G21/003C10G21/14C10G21/30G01D21/02
Inventor 廖志新罗涛王翠红佘玉成王红
Owner CHINA PETROLEUM & CHEM CORP
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com