Polyimide film, preparation method thereof and graphite film
A polyimide film and polyimide technology, applied in chemical instruments and methods, inorganic chemistry, non-metallic elements, etc., can solve the problems of reducing the heat dissipation effect, improve appearance, facilitate gas dissipation, free body base big effect
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[0022] One embodiment of the present application also provides a method for preparing a polyimide film, which includes the following steps:
[0023] Adding the diamine monomer, the dianhydride monomer and the catalyst into an organic solvent, stirring and reacting under a nitrogen atmosphere to obtain a polyamic acid solution;
[0024] Carrying out imidization treatment to the polyamic acid solution to obtain a polyimide solution;
[0025] Coating the polyimide solution on a support plate to obtain a polyimide coating film;
[0026] The polyimide film is baked and cured to obtain the polyimide film.
[0027] The polyimide solution includes the polyimide polymer and the organic solvent, and the polyimide polymer is dissolved in the organic solvent. In some embodiments, the organic solvent accounts for 80-85% by weight of the polyimide solution, in other words, the polyimide solution has a solid content of 15-20%.
[0028] It can be understood that the polyamic acid solution ...
Embodiment 1
[0036] Add diamine ENPSDA (0.1mol, 44.22g), catalyst (0.015g), dianhydride ODPA (0.1mole, 31.02g) and solvent NMP (300.97g) into a 500ml reaction flask to obtain a mixture with a solid content of 15-20%. The solution was stirred for 5 hours under a nitrogen atmosphere, then 60.2 g of xylene (Xylene) was added, and the temperature was raised to 190-200° C. and stirred for 15 hours under a nitrogen atmosphere to carry out dehydration and cyclization to obtain a polyimide solution.
Embodiment 2
[0038]Add diamine ENPSDA (0.09mol, 39.80g), diamine ODA (0.01mol, 2.0g), catalyst (0.015g), dianhydride ODPA (0.1mole, 31.02g) and solvent NMP (291.30g) into a 500ml reaction flask ) to obtain a mixed solution with a solid content of 15 to 20%, stirred for 5 hours under a nitrogen atmosphere, then added 58.30 g of xylene (Xylene), and heated up to 190 to 200° C. and stirred for 15 hours under a nitrogen atmosphere to carry out a water removal ring to obtain a polyimide solution.
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