Novel soft and smooth silicone oil for polyester and preparation method of novel soft and smooth silicone oil

A polyester and silicone oil technology, applied in fiber types, textiles and papermaking, fiber processing, etc., can solve problems such as poor hand feel and polyester fabrics that are not soft and slippery, and achieve the effect of improving soft and slippery performance.

Active Publication Date: 2022-05-27
浙江联胜新材股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The purpose of the present invention is to provide a new type of soft and slippery silicone oil for polyester and its prepar...

Method used

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  • Novel soft and smooth silicone oil for polyester and preparation method of novel soft and smooth silicone oil
  • Novel soft and smooth silicone oil for polyester and preparation method of novel soft and smooth silicone oil
  • Novel soft and smooth silicone oil for polyester and preparation method of novel soft and smooth silicone oil

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] The raw materials of the following metered weights are provided: polyether amine with a molecular weight of 600: 4.6 parts, diethyl terephthalate: 2 parts, epoxy-terminated polyether silicone oil with a molecular weight of 13000: 26.8 parts, ethylene glycol monobutyl ether: 28 parts , glacial acetic acid: 0.5 parts, deionized water 32.3 parts.

[0028] The specific preparation process of the soft and slippery silicone oil for polyester involved in the present invention is as follows:

[0029] (1) Add polyetheramine and diethyl terephthalate to the reactor, heat to 160°C, react for 5 hours and remove ethanol in a vacuum;

[0030] (2) Add epoxy-terminated polyether silicone oil and organic solvent to the reaction vessel, react at 100°C for 15 hours, cool to 50°C, and proceed to the next step;

[0031] (3) Slowly add 10 parts of deionized water, stir for 10 minutes, then mix the organic acid and 10 parts of deionized water evenly, and slowly add;

[0032] (4) Slowly add ...

Embodiment 2

[0034] The raw material of following measurement weight is provided: the polyether amine of molecular weight 600: 3.8 parts, diethyl terephthalate: 1.4 parts, the end epoxy polyether silicone oil of molecular weight 10000: 20 parts, ethylene glycol butyl ether: 25 parts, Glacial acetic acid: 0.5 parts, 49.5 parts of deionized water.

[0035] The specific preparation process of the soft and slippery silicone oil for polyester involved in the present invention is as follows:

[0036] (1) Add polyetheramine and diethyl terephthalate to the reactor, heat to 160°C, react for 6 hours and remove ethanol in a vacuum;

[0037] (2) Add epoxy-terminated polyether silicone oil and solvent to the reaction vessel, react at 100°C for 18 hours, cool to 50°C, and proceed to the next step;

[0038] (3) Slowly add 10 parts of deionized water, stir for 10 minutes, then mix the organic acid and 10 parts of deionized water evenly, and slowly add;

[0039] (4) Slowly add the remaining deionized wa...

Embodiment 3

[0041] The raw materials of the following metered weights are provided: polyether amine with a molecular weight of 900: 5.5 parts, diethyl terephthalate: 1.7 parts, epoxy-terminated polyether silicone oil with a molecular weight of 8000: 30.3 parts, butyl glycol ether: 30 parts, Glacial acetic acid: 0.5 parts, deionized water 32.0 parts.

[0042] The specific preparation process of the soft and slippery silicone oil for polyester involved in the present invention is as follows:

[0043] (1) Add polyetheramine and diethyl terephthalate to the reactor, heat to 160°C, react for 6 hours and remove ethanol in a vacuum;

[0044] (2) Add epoxy-terminated polyether silicone oil and solvent into the reaction vessel, react at 100°C for 24 hours, cool to 50°C, and proceed to the next step.

[0045] (3) Slowly add 10 parts of deionized water, stir for 10 minutes, then mix the organic acid and 10 parts of deionized water evenly, and slowly add;

[0046] (4) Slowly add the remaining deion...

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Abstract

The invention discloses novel soft and smooth silicone oil for polyester and a preparation method of the novel soft and smooth silicone oil. The novel soft and smooth silicone oil comprises the following raw materials in parts by mass: 2-10 parts of polyether amine, 1-5 parts of diethyl terephthalate, 10-30 parts of epoxy-terminated silicone oil, 10-30 parts of an organic solvent, 0.1-0.3 part of organic acid and 30-50 parts of deionized water. According to the novel soft and smooth silicone oil for terylene adopting the structure and the preparation method of the novel soft and smooth silicone oil, special polyether amine is prepared through amidation of diethyl terephthalate and polyether amine, epoxy-terminated polyether siloxane with medium and small molecular weight and the special polyether amine are subjected to polycondensation, and the prepared soft and smooth silicone oil for terylene can endow various terylene fabrics with softness, elasticity and elasticity. The handfeel is soft, smooth and fine.

Description

technical field [0001] The invention relates to the technical field of textile dyeing and finishing, in particular to a novel soft and smooth silicone oil for polyester and a preparation method thereof. Background technique [0002] Polyester fabric is a kind of chemical fiber clothing fabric widely used in daily life. It has the advantages of good elasticity, good heat resistance, good wear resistance, good light resistance, corrosion resistance, and high strength of polyester fabric. However, the disadvantages of polyester fabrics are also obvious. It is uncomfortable to wear, and the hard fibers will rub against the skin. In recent years, more and more polyester velvet fabrics are used in daily life, such as chiffon fabrics for summer women's clothing, which require a soft and silky feel; or fabrics such as polyester coral fleece, polyester flannel, polyester super soft, etc. , is used to make winter pajamas, winter bedding, etc. The more close-fitting the material is, ...

Claims

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Application Information

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IPC IPC(8): D06M15/65D06M101/32
CPCD06M15/652D06M2101/32D06M2200/50
Inventor 李兵涂胜宏谭函彬
Owner 浙江联胜新材股份有限公司
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