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Preparation method of easy-to-char EVA flame-retardant composite material

A flame retardant composite material and carbon-forming technology, applied in the field of EVA flame retardant materials, can solve the problems of high raw material cost, complicated operation, environmental pollution, etc., and achieve excellent oxygen index and mechanical properties, simple operation steps, and high flame retardant grade. Effect

Pending Publication Date: 2022-07-22
GREEN IND INNOVATION RES INST OF ANHUI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The purpose of this invention is to provide a kind of preparation method of easy-to-char EVA flame-retardant composite material, to solve the complex operation, high cost of raw materials, environmental pollution, easy to cause harm and the preparation of existing EVA flame-retardant composite material in the prior art. The problem of the decline in the mechanical properties of the finished product

Method used

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  • Preparation method of easy-to-char EVA flame-retardant composite material
  • Preparation method of easy-to-char EVA flame-retardant composite material
  • Preparation method of easy-to-char EVA flame-retardant composite material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] 1. In Example 1, the flame retardant is magnesium hydroxide, the addition amount is 57%, the compatibilizer is MC226, the addition amount is 4.8%, the antioxidant is antioxidant 1010, the additive is 0.2%, and the synergist is The addition amount of triphenylphosphine oxide is 3%. The above materials and EVA (addition amount of 35%) are put into an internal mixer together, and mixed at 150 ° C for 10 minutes.

[0033] 2. Take out the kneaded product in step 1 and place it on a flat vulcanizer for hot pressing molding, with a pre-pressing time of 1 min, a pressing time of 10 min, and a hot-pressing temperature of 170°C.

[0034] 3. Cut the composite material in step 2 to the required size.

[0035] 4. Take the spline cut in step 3 for testing.

Embodiment 2

[0037] 1. In this example 1, the flame retardant is magnesium hydroxide, the addition amount is 57%, the compatibilizer is MC226, the addition amount is 4.8%, the antioxidant is antioxidant 1010, the additive is 0.2%, and the synergist is 3000 mesh silicon powder, the addition amount is 3%. The above materials and EVA (addition amount of 35%) were put into the internal mixer together, and mixed at 150 ° C for 10 min.

[0038] 2. Take out the kneaded product in step 1 and place it on a flat vulcanizer for hot pressing. The pre-pressing time is 1 min, the pressing time is 10 min, and the hot-pressing temperature is 170°C.

[0039] 3. Cut the composite material in step 2 to the required size.

[0040] 4. Take the spline cut in step 3 for testing.

Embodiment 3

[0042] 1. In this example 1, the flame retardant is magnesium hydroxide, the addition amount is 57%, the compatibilizer is MC226, the addition amount is 4.8%, the antioxidant is antioxidant 1010, the additive is 0.2%, and the synergist is Silicone powder, the addition amount is 3%. The above materials and EVA (addition amount of 35%) were put into the internal mixer together, and mixed at 150 ° C for 10 min.

[0043] 2. Take out the kneaded product in step 1 and place it on a flat vulcanizer for hot pressing. The pre-pressing time is 1 min, the pressing time is 10 min, and the hot-pressing temperature is 170°C.

[0044] 3. Cut the composite material in step 2 to the required size.

[0045] 4. Take the spline cut in step 3 for testing.

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Abstract

The invention discloses a preparation method of an easy-to-char EVA flame-retardant composite material, the composite material comprises 20-40% of EVA, 3-10% of a compatilizer, 0.05-0.3% of an antioxidant, and 50-70% of a flame retardant and a synergist, the mass ratio of the flame retardant to the synergist is 55: 5-59: 1, and during manufacturing, the components are mixed and hot-pressed to obtain a finished product. The EVA flame-retardant composite material disclosed by the invention is combusted to generate a more compact carbon layer, so that a better flame-retardant effect is achieved. The manufacturing method is simple in operation steps and low in cost, and meets the green chemistry concept and national environmental protection requirements.

Description

technical field [0001] The invention relates to the field of EVA flame retardant materials, in particular to a preparation method of an EVA flame retardant composite material that is easy to form carbon. Background technique [0002] my country's demand for cables is increasing. EVA (ethylene-vinyl acetate copolymer) is widely used in adhesives, cables and sports because of its high transparency, soft texture, easy manufacture, controllable structure and good environmental resistance. It is widely used in many fields such as equipment. However, due to the low ignition point of EVA due to its own structure, and the combustion is accompanied by a large amount of smoke, it is often necessary to add flame retardants to enhance the flame retardant effect. [0003] At present, the commonly used inorganic flame retardants on the market are aluminum hydroxide and magnesium hydroxide. The flame retardant mechanism is that metal hydroxides will decompose to produce water and metal oxi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L23/08C08K3/22C08K5/5397C08K3/36C08L83/04
CPCC08L23/0853C08K2003/2224C08L2201/02C08K3/22C08K5/5397C08K3/36C08L83/04
Inventor 刘志启吴青山赵鹏程夏子璐胡丽娟唐涛刘丽芳李一览陈宇楠昝兴杰
Owner GREEN IND INNOVATION RES INST OF ANHUI UNIV