Ternary positive electrode material conductive paste using graphene and preparation method of ternary positive electrode material conductive paste
A technology of conductive paste and positive electrode material, which is applied to conductive materials dispersed in non-conductive inorganic materials, cable/conductor manufacturing, circuits, etc. The effect of battery internal resistance, energy density improvement, and stress relief
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[0025] The present application also provides a method for preparing the above-mentioned ternary positive electrode material conductive paste, including the following steps: using N-methylpyrrolidone to dissolve polyvinylidene fluoride, conductive carbon black and graphene to prepare a first solution. A second solution was prepared by dissolving the carbon nanotubes using N-methylpyrrolidone and a dispersant. The first solution and the second solution are mixed to a viscosity of 1450-1550 mPa.s to prepare a conductive paste.
[0026] Wherein, the first solution was prepared using N-methylpyrrolidone in 50% of the formula. A second solution was prepared using a 50% formulation amount of N-methylpyrrolidone.
[0027] After the first solution and the second solution are mixed, a homogenizer is used for thorough stirring, and the final viscosity is 1450-1550 mPa.s. Preferably, the viscosity is 1500 mPa.s.
[0028] In addition, the conductive paste should be stored in a low-tempe...
Embodiment 1
[0031] formula:
[0032] According to 100 g per part by weight, 0.0001 part by weight of graphene, 0.5 part by weight of carbon nanotube, 1 part by weight of polyvinylidene fluoride, 3.5 part by weight of conductive carbon black, 95 part by weight of N-methylpyrrolidone, and 0.015 part by weight of dispersant.
[0033] making process:
[0034] The first solution is prepared by dissolving polyvinylidene fluoride, conductive carbon black and graphene with N-methylpyrrolidone in 50% of the formula. A second solution was prepared by dissolving the carbon nanotubes using 50% of the formulation amount of N-methylpyrrolidone and a dispersant. The first solution and the second solution are mixed, and then fully stirred with a homogenizer to finally reach a viscosity of 1500 mPa.s to prepare a conductive paste.
[0035] After the conductive paste of this embodiment is mixed with a 2.5-micron ternary material, the energy density of the battery is 180 mA·h / g, and the number of cycles i...
Embodiment 2
[0037] formula:
[0038] According to 100 g per part by weight, 0.0005 part by weight of graphene, 0.5 part by weight of carbon nanotube, 1 part by weight of polyvinylidene fluoride, 3.5 part by weight of conductive carbon black, 95 part by weight of N-methylpyrrolidone, and 0.015 part by weight of dispersant.
[0039] making process:
[0040] The first solution is prepared by dissolving polyvinylidene fluoride, conductive carbon black and graphene with N-methylpyrrolidone in 50% of the formula. A second solution was prepared by dissolving the carbon nanotubes using 50% of the formulation amount of N-methylpyrrolidone and a dispersant. The first solution and the second solution are mixed, and then fully stirred with a homogenizer to finally reach a viscosity of 1500 mPa.s to prepare a conductive paste.
[0041] After mixing the conductive paste of this embodiment with a ternary material of 3 microns, the energy density of the battery is 193 mA·h / g, and the number of cycles i...
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