Recovery of tin from waste liquid of tin and lead
A waste liquid and tin-lead technology, applied in the field of tin recycling, can solve the problems of waste of limited resources, secondary environmental pollution, heavy metal transfer, etc., achieve significant economic benefits, and solve the effect of secondary pollution of heavy metals
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[0044] An implementation process step of the present invention is:
[0045] (1) Distill under reduced pressure on the printed circuit board tin stripping waste liquid to two-thirds of the volume of the original liquid, temperature 75℃, pressure 0.5×1.03×10 5 Pa;
[0046] (2) Add NaOH to the waste liquid after distillation for neutralization, and control the pH value of the neutralization solution to 6-8;
[0047] (3) Filter the aforementioned neutralized waste liquid in a conventional manner to obtain a filter cake;
[0048] (4) Add NaOH to the resulting filter cake and heat it to 120°C for alkali dissolution until it is completely dissolved;
[0049] (5) Hot-dip the alkali solution for 4 hours, temperature 95°C, alkali (NaOH) concentration 200g / L, and the liquid-solid ratio of water to filter cake by weight is 6;
[0050] (6) The hot immersion liquid is routinely filtered, and the corresponding amount of Na is added to the filtrate 2 S in addition to impurities;
[0051] (7) Afte...
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