High-alkalization degree poly-ion polymerized composite coagulant and preparation method thereof
A technology of alkalinity and polyion, applied in the direction of flocculation/sedimentation water/sewage treatment, etc., can solve the problems of limitation, low content of heavy metal impurities, high product cost, and achieve the effect of reducing maintenance costs, improving conversion rate and saving energy.
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Embodiment 1
[0019] Weigh aluminum hydroxide: 1.366 tons; hydrochloric acid: 6.898 tons, heat up to 130°C, pressure 0.15MPa, and react for 2 hours. Add 5.09 tons of water to the reaction tank, add the above-mentioned feed liquid, the temperature should be between 70-90°C, add 2.40 tons of calcium powder for reaction, when the viscosity of the reaction feed liquid reaches 102-103mPa·S, some water can be added Dilute and continue to react. When the viscosity of the feed liquid reaches the initial viscosity again, add some water to dilute again, and repeat this for 2 to 3 times until the viscosity of the feed liquid reaches between 10mPa·S and 300mPa·S, and the viscosity of the feed liquid no longer continues Finally, add all the remaining 3.5 to 4.5 tons of water into the feed liquid at one time, and this process should be completed within 2 hours. A total of 5.8 tons of water was added during the reaction, and the temperature of the feed liquid after adding calcium powder should be kept bet...
Embodiment 2
[0021] Weigh aluminum hydroxide: 1.466 tons; hydrochloric acid: 6.40 tons, heat up to 150°C, pressure 0.20MPa, and react for 1.5 hours. Add 4.50 tons of water to the reaction tank, add the above-mentioned feed liquid, the temperature should be between 70-90°C, add 2.50 tons of calcium powder for reaction, when the viscosity of the reaction feed liquid reaches 102-103mPa·S, add some water Dilute and continue to react. When the viscosity of the feed liquid reaches the initial viscosity again, add some water to dilute again, and repeat this for 2 to 3 times until the viscosity of the feed liquid reaches between 10mPa·S and 300mPa·S, and the viscosity of the feed liquid no longer continues Finally, add all the remaining 4 to 5 tons of water into the feed liquid at one time, and this process should end within 1.5 hours. A total of 6.50 tons of water was added during the reaction, and the temperature of the feed liquid after adding calcium powder should be kept between 50 and 70°C. ...
Embodiment 3
[0023] Weigh aluminum hydroxide: 1.628 tons; hydrochloric acid: 6.4 tons, add 4.8 tons of water to the reaction tank, add the above-mentioned liquid, the temperature should be between 70 ~ 90 ° C, add 2.60 tons of calcium powder for reaction, when the reaction material When the viscosity of the liquid reaches 102-103mPa·S, add part of water to dilute and continue the reaction. When the viscosity of the material liquid reaches the initial viscosity again, add part of water to dilute again, and repeat this for 2-3 times until the viscosity of the material liquid reaches 10mPa·S Between ~300mPa·S, until the feed liquid is no longer viscous, finally add all the remaining 5-6 tons of water into the feed liquid at one time, and this process should end within 1.5 hours. A total of 7.0 tons of water was added during the reaction, and the temperature of the feed liquid after adding calcium powder should be kept between 50 and 70°C.
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