Method of producing electrode for capacitor
A manufacturing method and capacitor technology, which is applied in hybrid capacitor electrodes, hybrid/electric double-layer capacitor manufacturing, capacitors, etc., can solve problems such as the difficulty of thinning the electrode layer, and achieve the effect of realizing light weight and miniaturization
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Embodiment 1
[0078] (Preparation of coating liquid for inner coating)
[0079] 60 g of acetylene black (manufactured by Denka Kogyo Co., Ltd., trade name: denka black, BET specific surface area: 67m 2 / g), and 40 g of fluororubber (manufactured by Dupon Corporation, trade name: Viton-GF) were dropped into 186 g of methyl isobutyl ketone (MIBK), and mixed for 45 minutes using a planetary mixer, and the mixture was further mixed. 964 g of MIBK was added and stirred for 1 hour to obtain a slurry. The obtained slurry was put into a sand mill, and zirconia beads (manufactured by Nichikato-Co., Ltd., zirconia ZrO 2 , particle size: 0.3 mm), the residence time is 2 minutes of dispersion treatment. In addition, at this time, the peripheral speed of the disperser was 10 m / sec, the flow rate was 138 g / min (160 ml / min), and the bead filling rate was 80% by weight. In this way, a coating liquid for an undercoat layer was prepared. The coating liquid for an undercoat layer maintains a good dispersi...
Embodiment 2~7、 comparative example 1
[0102] In addition to changing the drying conditions of the electrode coating layer as shown in Table 1, and respectively changing the amount of residual solvent in the entire layer (both inner coating layers + both electrode coating layers) after drying as shown in Table 1, In the same manner as in Example 1, an electrode for an electric double layer capacitor was produced. For each of the obtained electrodes, the measurement of the electrode density was performed, and the determination of contamination of the guide roller was also performed. The results are shown in Table 1.
[0103] Electrode Coating Layer
[0104] As can be seen from Table 1, the electrodes obtained in Examples 1 to 7 of the present invention have high electrode densities and are preferable. On the other hand, the electrode obtained in Comparative Example 1 was poor in electrode density. The amount of residual solvent in the entire layer after drying was as high as 37% by weight, and contamin...
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