Manufacture Process Of Non-Oriented Silicon Steel With High Magnetic Induction

a manufacturing process and non-oriented technology, applied in the direction of metal rolling arrangement, inorganic material magnetism, etc., can solve the problems of increasing electric loss in end use, weakening the magnetic induction of the sheet, and affecting the magnetic properties of non-oriented silicon steel, so as to improve the magnetic induction, improve the grain structure and texture, and improve the effect of grain growth

Inactive Publication Date: 2012-11-15
BAOSHAN IRON & STEEL CO LTD
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Benefits of technology

[0027]The intension to have the hot-rolled plate normalized and pre-annealed is to improve grain structure and texture. A research on non-oriented silicon Steel indicates that to make grain structure become coarse prior to cold-rolling can weaken texture component {111} of the cold-rolled sheet and can intensify texture component {ok1} of the cold-rolled sheet after it is finish-annealed, texture component {ok1} is advantageous to magnetic property. Moreover, the incidental phenomenon of separated substance becoming coarser can make grains grow up even easier so as to improve magnetic induction and reduce iron loss. In the invention, normalization temperature of high-magnetic-induction non-oriented silicon steel plate is not below 950° C., soakage period is 30˜180s.
[0028]The grains of {110} Gauss texture which are advantageous to magnetic property are usually to nucleate and grow up in the shear-deformed zone of the cold-rolled material. If temperature rise rate is too low, in the phase of temperature being lower, a recovery process in material will occur, which will reduce lattice distortion, thus, the probability of Gauss texture to nucleate will greatly fall down. To use a high temperature rise rate in annealing procedure can rapidly go through the temperature range adverse to evolution of Gauss texture and can make the surface texture {ok1} advantageous to magnetic property evolute even better, and thereby, can optimize magnetic induction and iron loss. To cool the annealed sheet slowly can improve its magnetic property. In the invention, the cold-rolled sheet is finish-annealed by quickly heating to a temperature between 800˜1000° C. at a temperature rise rate of ≧100° C. / s and a soakage period of 5˜60s, thereafter, is slowly cooled to 600˜750° C. at cooling rate of 3˜15° C. / s.
[0029]In comparison to conventional manufacture processes, the manufacture process of the invention can raise magnetic induction of non-oriented silicon Steel by at least 200 Gauss under the precondition to maintain the same iron loss.

Problems solved by technology

The magnetic properties of non-oriented silicon Steel are very prone to be affected by various factors such as material compositions, thickness, heat treatment procedure, and so on.
If soakage temperature is too high and soakage period is too long, the crystal grains of annealed silicon Steel will be rather coarse, the surface texture {111} will be intensified, and magnetic induction of the sheet will be weakened; contrarily, if diameters of the grains are on the small side, the hysteresis loss of material will be on the large side, which will increase electric loss in end use.
In anneal procedure, as compared to heating at a lower temperature rise rate, heating at a higher temperature rise rate will bring about quite intensive Gauss texture.

Method used

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  • Manufacture Process Of Non-Oriented Silicon Steel With High Magnetic Induction

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Experimental program
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embodiment 1

[0032](1) Hot-rolled non-oriented silicon steel plate with 2.6 mm thickness, its compositions and their contents are: Si 0.799%, Al 0.4282%, C 0.0016%, Mn 0.26%, P≦0.022%, S≦0.0033%, N≦0.0007%, Nb 0.0004%, V 0.0016%, Ti 0.0009%, the rest is Fe and unavoidable inclusions.

[0033](2) The hot-rolled plate is cold-rolled at a compression ratio of 1˜10%.

[0034](3) The cold-rolled plate is normalized at normalization soakage temperature of 970° C. and maintained at the temperature for 60s, thereafter the normalized plate is pickled, and then, cold-rolled into a Steel of 0.5 mm thickness.

[0035](4) the cold-rolled sheet is annealed at a high heating rate in an electric annealing furnace in a laboratory, with temperature rise rate of 250° C. / s, soakage temperature of 850° C. and soakage time of 13s.

[0036]It is found that in the case of the hot-rolled plate being cold-rolled at a compression ratio of 1˜10%, the re-crystallized grains of the normalized sheet after being normalized become clearly ...

embodiment 2

[0038](1) Hot-rolled non-oriented silicon steel plate with 2.6 mm thickness, its compositions and their contents are: Si 1%, Al 0.2989%, C 0.0015%, Mn 0.297%, P 0.0572%, S 0.0027%, N 0.0009%, Nb 0.0005%, V 0.0015%, Ti 0.0011%, the rest is Fe and unavoidable inclusions.

[0039](2) The hot-rolled plate is cold-rolled at rolling compression ratio of 4%.

[0040](3) The cold-rolled plate is normalized at normalization soakage temperature of 950° C. and maintained at the temperature for 60s, thereafter, the normalized plate is pickled, and then cold-rolled into a Steel of 0.5mm thickness.

[0041](4) the cold-rolled sheet is annealed at a high heating rate in an electric annealing furnace in a laboratory, with different temperature rise rates of 20° C. Is, 150° C. / s and 250° C. Is, respectively, soakage temperature of 960° C. and soakage time of 13s.

[0042]The magnetic property of the finish-annealed sheet is shown in Table 3.

TABLE 3magnetic property of the finish-annealed non-oriented silicon St...

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Abstract

A manufacture process of non-oriented silicon steel with high magnetic induction includes smelting and casting steel having a chemical composition by weight percent: Si 0.1˜1%, Al 0.005˜1.0%, C≦0.004%, Mn=0.10˜1.50%, P≦0.2%, S≦0.005%, N≦0.002, Nb+V+Ti≦0.006%, and the rest is Fe. The steel is cast into a billet, which is heated and hot-rolled to 1150˜1200° C. into a plate at a finish-rolling temperature 830˜900° C. The plate is cooled to a temperature ≧570° C. and cold-roll flattened at compression ratio 2˜5%. The flattened plate is normalized at temperature not below 950° C. for 30˜180s, and then pickled and cold-rolled into a sheet with thickness of the finished product. The sheet is finish-annealed quickly heating the sheet to 800˜1000° C. at temperature rise rate ≧100° C./s, soaking the heated sheet for 5˜60s at the temperature, and then slowly cooling the sheet to 600˜750° C.

Description

CROSS REFERENCE TO RELATED APPLICATIONS[0001]The present application is a continuation of PCT Patent Application No. PCT / CN2011 / 072775 filed on Apr. 14, 2011, which claims priority to Chinese Patent Application No. 201010517872.7 filed on Oct. 25, 2010, both of which are fully incorporated herein by reference.STATEMENT REGARDING FEDERALLY SPONSORED RESEARCH OR DEVELOPMENT[0002]Not applicable.FIELD OF THE INVENTION[0003]This invention relates generally to a manufacture process of non-oriented silicon Steel, and particularly, to a manufacture process of non-oriented silicon Steel with high magnetic induction.BACKGROUND OF THE INVENTION[0004]Non-oriented silicon Steel is an important magnetic material and widely used in manufacture of various electric machines, compressors and so on. In general, it contains silicon of less than 6.5%, aluminum of less than 3%, carbon of less than 0.1%, and other trace elements. Manufacture process of silicon Steel includes the procedures of hot-rolling,...

Claims

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Application Information

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Patent Type & Authority Applications(United States)
IPC IPC(8): C21D8/00
CPCC22C38/00C22C38/02C22C38/06C21D6/008C21D8/00C21D1/00H01F1/16C22C38/002C22C38/004C22C38/04C22C38/12C22C38/14C22C38/001B21B1/00B22D11/00
Inventor WANG, ZITAOWANG, BOXIE, SHISHUJIN, BINGZHONGMA, AIHUAZOU, LIANGZHU, YUHUAHU, ZHANYUANCHEN, XIAO
Owner BAOSHAN IRON & STEEL CO LTD
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