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84results about How to "Reduce lattice distortion" patented technology

Copper chromium zirconium alloy and preparing method thereof

A copper chromium zirconium alloy comprises, by weight, 0.7% to 2.0% of chromium, 0.05% to 0.3% of zirconium, 0.01% to 0.08% of magnesium, 0.01% to 0.1% of yttrium and the balance copper. The invention further provides a preparing method of the copper chromium zirconium alloy. The preparing method sequentially comprises the following steps that firstly, the copper, the chromium, the zirconium, the magnesium and the yttrium are prepared according to the proportion and are subject to vacuum purified smelting and flow dividing type casting, and a casting blank is prepared; secondly, the casting blank is subject to homogenization treatment and hot extrusion, and a sheared billet is prepared; thirdly, the sheared billet is subject to solid-solution treatment; fourthly, the sheared billet obtained after the solid-solution treatment is subject to cold deformation machining; and fifthly, a material obtained after cold deformation machining is subject to aging treatment, and the needed copper chromium zirconium alloy is obtained. The copper chromium zirconium alloy has the good comprehensive performance, the room temperature tensile strength of the copper chromium zirconium alloy is larger than 520 MPa, the room temperature elongation of the copper chromium zirconium alloy is larger than or equal to 22%, the room temperature electric conductivity of the copper chromium zirconium alloy is larger than or equal to 90%IACS, and the 350 DEG C high-temperature tensile strength of the copper chromium zirconium alloy is larger than 390 MPa.
Owner:SHANTOU HUAXING (RAOPING) COPPER IND CO LTD +1

Thin-film solar photovoltaic cell with nano wire array structure and preparation method for thin-film solar photovoltaic cell

The invention discloses a method for preparing a thin-film solar photovoltaic cell with a copper indium gallium selenide (CIGS) nano wire array structure. The method comprises the following steps of: growing a large-area cuprous sulfide or copper sulfide nano wire array by adopting a gas-solid reaction method, and converting the cuprous sulfide or copper sulfide nano wire array into a CIGS nano wire array by physical vapor deposition and heat treatment methods. The component, the phase structure and the energy band structure of the semiconductor nano wire array can be regulated by controlling the categories of deposition elements, the deposition sequence, the deposition process, post treatment and the like, so that solar photovoltaic cells with different structures and properties are prepared. Through the cell, light reflection is reduced, light absorption is increased, the probability of producing current carriers can be increased, the probability of recombination of holes and electrons is reduced, and the photoelectric conversion efficiency is greatly improved. The method is low in cost, the preparation processes are controllable, the prepared nano wire array is uniform in structure distribution, and preparation of the nano structural thin-film solar photovoltaic cell with large area and high photoelectric conversion efficiency can be realized.
Owner:SUN YAT SEN UNIV

Aluminum or aluminum alloy conductor twisting and compressing process for cables

The invention provides an aluminum or aluminum alloy conductor twisting and compressing process for cables. The aluminum or aluminum alloy conductor twisting and compressing process comprises the following steps of: twisting aluminum or aluminum alloy single wires along the traction direction of the aluminum or aluminum alloy single wires; and compressing the twisted aluminum or aluminum alloy single wires by a compression roller, wherein a layer of twisting layer is formed after the aluminum or aluminum alloy single wires are twisted once and compressed by means of the compression roller, the subsequent twisting layer is twisted on the basis of the fore twisting layer, and the twisting direction of the last twisting layer is the same as that of the second last twisting layer. According to the aluminum or aluminum alloy conductor twisting and compressing process, the twisting directions of the outermost two layers of twisting layers are the same, the compression roller is combined with a nano diamond composite coating compression die, the phenomena of surface burrs of compressed round aluminum conductors, more aluminum scraps and wire fracture are prevented, the influence of alcohol which is continuously dripped for lubricating and cooling on the residual water inside or on the surface of the conductors is eliminated, the volume resistivity of the twisted and compressed cables is reduced by 0.5 to 2.0 percent, the production cost is saved, and the social benefit is higher.
Owner:SICHUAN MINGXING CABLE

Active ion controlled doping yttrium aluminum garnet base laser transparent ceramic material and preparation method thereof

The invention relates to an active ion controlled doping yttrium aluminum garnet base laser transparent ceramic material and a preparation method thereof. The method comprises the following steps of: (1) carrying out ball mill mixing on oxide ceramic powder body raw materials, sintering auxiliary agents, binding agents and absolute ethyl alcohol to prepare ethyl alcohol base slurry, wherein the slurry comprises the following ingredients through being metered by mass: 40 to 70 percent of oxide ceramic powder body raw materials, 0.01 to 1 percent of sintering auxiliary agents, 0 to 2.5 percent of binding agents and the balance absolute ethyl alcohol; (2) drying the ethyl alcohol base slurry prepared in the first step, then, carrying out sieving and granulation, or carrying out direct spray granulation on the slurry; (3) loading powder body spherical particles prepared in the second step through granulation into clean bags filled with air and uniformly mixing the powder body spherical particles; (4) directly pressing and forming the powder body spherical particles uniformly mixed in the third step or carrying out the pressing forming after the pre-calcination treatment; and (5) carrying out vacuum sintering on ceramic blanks prepared in the fourth step through pressing and forming, then, carrying out annealing and mechanical processing treatment and obtaining the active ion controlled doping yttrium aluminum garnet base laser transparent ceramic material.
Owner:中国科学院上海硅酸盐研究所苏州研究院

Centrifugal ceramic composite vertical mill roller sleeve and manufacturing method thereof

The invention discloses a centrifugal ceramic composite vertical mill roller sleeve and a manufacturing method thereof. The centrifugal ceramic composite vertical mill roller sleeve comprises an inner layer and an outer layer. The outer layer is high-chromium cast iron, and ceramic particles are embedded in the outer layer. The high-chromium cast iron is prepared from, by weight, 2.3-3.3% of C, 0.3-1.0% of Si, 0.6-1.2% of Mn, 18-22% of Cr, 0.7-1.7% of Ni, 1.5-3.0% of Mo, 0-0.03% of P, 0-0.03% of S and the balance Fe and inevitable impurities. According to the vertical mill roller sleeve, the material proportion of the inner layer and the outer layer is optimized; high-alloy elements are adopted by the outer layer, the matrix can be effectively reinforced by increasing the content of alloy such as C, Cr, Mo and V, the total amount of carbide is increased, and therefore the smoothness of a friction surface can be effectively improved; the outer layer of the roller sleeve is made to be high in abrasion resistance, high in strength and enough in toughness, and the service life of the roller sleeve is effectively prolonged. According to the manufacturing method, a heat treatment technique of annealing, quenching and tempering is adopted, the purposes of improving the carbide form, promoting structural transformation and refining structures are achieved, so that the abrasion resistance and fracture toughness of the roller sleeve are improved.
Owner:河北津西钢铁集团重工科技有限公司

Semi-solid state extrusion casting aluminum alloy for new energy automobile and preparation method thereof

The invention relates to a semi-solid state extrusion casting aluminum alloy for a new energy automobile and a preparation method thereof. The alloy comprises, by weight, 5%-8% of Si, 3.5%-4% of Cu, 0.40%-0.80% of Fe, 0.00%-0.5% of Mg, less than or equal to 0.05% of other impurities, and the balance Al. The alloy melt is subjected to 50Hz mechanical vibration treatment within the temperature interval of 650-680 DEG C, and semi-solid state slurry is obtained after 180-240 s. Compared with the prior art, the aluminum alloy provided by the invention has the solid-liquid phase interval of 510-630DEG C, thereby having the semi-solid state extrusion casting performance. The aluminum alloy melt starts to be subjected to 50Hz mechanical vibration treatment within the temperature interval of 650-680 DEG C, and the semi-solid state slurry can be obtained after 180-240 s. The slurry is subjected to extrusion casting, heat treatment at 450 DEG C for 2 h and artificial ageing at 170 DEG C for 10 h. Eutectic silicon particles are distributed densely. Al2Cu serves as a main precipitated phase in the material, and a small number of Al5Cu2Mg8Si6 and Al8Mg3FeSi2 are generated simultaneously. The aluminum alloy has the tensile strength greater than 420 MPa, the yield strength greater than 380 MPa and the heat conductivity coefficient greater than 160 W/m.K under the enhancement effect of the precipitated phase.
Owner:苏州慧驰轻合金精密成型科技有限公司

Novel production method of c-orientation sapphire single crystal

The invention discloses a novel production method of a c-orientation sapphire single crystal. The novel production method comprises the following steps of: placing c-orientation sapphire seed crystals in the seed crystal groove of a crucible; filling high-purity aluminum oxide raw materials; vacuumizing and subsequently heating to completely melt the aluminum oxide raw materials and partially melt the seed crystals; slowly cooling at a speed of 0.01-10DEG C / h; controlling a solid-liquid interface to a plane having a certain angle with a c-surface; annealing at a cooling speed of 2-50 DEG C / h after the growth of the crystals is ended; and cooling to the room temperature and subsequently taking the crystal out. According to the invention, by adopting a method for deviating a crucible symmetry axis, a heater symmetry axis and a lateral reflecting screen symmetry axis, the solid-liquid interface in the growth process of the sapphire single crystal is a plane having a certain angle with the c-surface, and the material utilization rate of grown c-orientation crystal ingots can be greatly improved in comparison with the material utilization rate of a-orientation crystal ingots; and compared with the traditional growth method of the c-orientation crystal ingots, the crystal quality of the crystal ingots can be improved and the distortions of crystal boundaries and crystal lattices normally occurring during the growth of the c-orientation crystal ingots can be reduced.
Owner:苏州海铂晶体有限公司

Magnetic field-induced preparation method of molecularly-imprinted magnetic enrichment material of trace quantity of chlorophenol pollutant molecules in seawater

InactiveCN104130441AAvoid easy reunionAvoid low magnetic contentOther chemical processesSeawater treatmentSolid phase extractionAmino functionalized
The invention discloses a magnetic field-induced preparation method of a molecularly-imprinted magnetic enrichment material of trace quantity of chlorophenol pollutant molecules in seawater. The preparation method comprises that under magnetic field induction, an epoxy group-functionalized magnetic polymer is prepared by suspension polymerization and in-situ oxidation, a chlorophenol environmental pollutant polyamine template molecule is obtained by an intermolecular hydrogen bonding self-assembling technology, an amino-functionalized magnetic molecularly-imprinted composite material bonding with the template molecule is prepared under magnetic field induction, and in the presence of an acid/alcohol extractant, through pH adjustment, the template molecule is eluted and the chlorophenol molecule-imprinted magnetic composite material is obtained. The preparation method has simple processes and a low cost and realizes uniform particle size distribution and stable properties of the desired product. The molecularly-imprinted magnetic enrichment material can realize high-efficiency and high-selectivity adsorption and removal of trace quantity of chlorophenol pollutants in seawater and can be used for base dispersion-magnetic solid phase extraction detection of trace quantity of chlorophenol pollutants in seawater.
Owner:NINGBO INST OF TECH ZHEJIANG UNIV ZHEJIANG

Inert transition metal element doped iron-based Prussian blue sodium ion battery positive electrode material

The invention relates to an inert transition metal element doped iron-based Prussian blue sodium ion battery positive electrode material and a preparation method thereof, wherein an inert transition metal element zinc Zn is used for replacing high spin iron connected with N in cyanide in iron-based Prussian blue according to a certain proportion. The preparation method comprises the following steps: dissolving ferrous sulfate heptahydrate, zinc acetate and sodium citrate in deionized water to form a solution A, dissolving sodium ferrocyanide decahydrate and ascorbic acid in deionized water to form a solution B, and dissolving polyvinylpyrrolidone and sodium chloride in deionized water to form a solution C; simultaneously adding the solution A and the solution B into the solution C through a peristaltic pump, and stirring while heating in an N2 atmosphere until the solution becomes white suspension liquid after dropwise adding is completed, namely, a solution D; and continuously stirring the solution D under the same condition, finally aging at room temperature, then centrifugally washing with deionized water and absolute ethyl alcohol three times respectively, and carrying out vacuum drying to obtain the zinc-doped iron-based Prussian blue Zn-FeHCF positive electrode material.
Owner:CHINA THREE GORGES UNIV

Micro/nanometer secondary surface array and preparation method and application thereof

The invention discloses a 'cactus' micro / nanometer secondary surface array structure, a preparation method and application of the 'cactus' micro / nanometer secondary surface array structure. The micro / nanometer secondary surface array is formed in the manner that nanoscale copper 2 sulphur (Cu2S) nanometer lines grow on the surface of micron scale Cu2S spherical crowns, and the Cu2S spherical crowns are periodically distributed on the surface of a substrate. Compared with a common plane nanometer line array, the Cu2S'cactus' micro / nanometer secondary surface array further increases specific surface area, and increases probability of generation of charge carriers. Meanwhile, when the angle of incident light changes, change of relative position between the nanometer lines and light rays is small, and change of light absorption is small, so the light absorption can maintain good performance within the wide light incident angle. When the Cu2S'cactus' micro / nanometer secondary surface array is applied to the field of solar energy, the Cu2S'cactus' micro / nanometer secondary surface array can overcome the defects of degrading the performance along with the position of the sun, or changing angles of devices continuously along with the change of illumination angles to cause complexity of structure of the devices and increase of cost.
Owner:SUN YAT SEN UNIV

Chain-like nanometer magnetic material, preparation method and application thereof

The invention discloses a chain-like nanometer magnetic material, a preparation method and an application thereof. The chain-like nanometer magnetic material is characterized by containing the following raw materials: ferric iron, acetate, dispersing agent and organic amine or organic acid; the mass concentrations of the ferric iron and the acetate in the dispersing agent are respectively 5-500g/L and 10-800g/L; the mass concentration of the organic amine or organic acid in the mixed solution after adding is 1-800g/L. According to the invention, various organic acids and organic amine are expanded; an amino or carboxyl modified chain-like nanometer magnetic composite material is acquired through a one-step process; the material with the chain-like structure can be acquired in the manner of inducing the composite material through hydrogen bond and magnetic field; the invention obviously innovates the controllability of the aggregation state structure of the material. The traditional method is performed in multiple steps, a covalent organic frame magnetic composite microsphere with a porous structure is acquired, the preparation process of the material is complex, the nonmagnetic components of the material are increased, the magnetic content of the acquired material is reduced and the method is adverse to magnetic separation.

1000MPa-grade high-toughness and high-magnetism hot-rolled magnetic yoke steel and production method thereof

The invention discloses 1000MPa-grade high-toughness and high-magnetism hot-rolled magnetic yoke steel and a production method thereof. The 1000MPa-grade high-toughness and high-magnetism hot-rolled magnetic yoke steel is prepared from the following components in percentage by weight: 0.20 to 0.50 percent of C, 0.2 to 1.0 percent of Si, 0.5 to 1.5 percent of Mn, less than or equal to 0.015 percentof P, less than or equal to 0.005 percent of S, less than or equal to 0.06 percent of Ti, less than or equal to 0.05 percent of Nb, 0.20 to 1.0 percent of Mo, 0.20 to 1.20 percent of Cr, 0.20 to 0.60percent of Ni, 0.03 to 0.15 percent of V, 0.0005 to 0.003 percent of B, 0.015 to 0.10 percent of Al, less than or equal to 0.010 percent of N, less than or equal to 0.0080 percent of O, and the balance of Fe and other unavoidable impurities; and meanwhile Cr+Mo+Ni is larger than or equal to 0.80 percent; Nb+V+Ti is larger than or equal to 0.06 percent; carbon equivalent CEV is larger than or equal to 0.50 percent. The yield strength of the hot-rolled magnetic yoke steel is larger than or equal to 1000MPa, the tensile strength is larger than or equal to 1050MPa; the impact power KV<2> is larger than or equal to 40J at the temperature of 20 DEG C below zero; the magnetic induction performance B<50> is larger than or equal to 1.58T; B<100> is larger than or equal to 1.73T; B<200> is larger than or equal to 1.90T; and B<300> is larger than or equal to 1.93T. The 1000MPa-grade high-toughness and high-magnetism hot-rolled magnetic yoke steel meets relevant requirements of the hydropower industry on rotor magnetic yoke steel.
Owner:BAOSHAN IRON & STEEL CO LTD

Antifriction lead-free copper-based sliding bearing material and preparation method thereof

The invention discloses an antifriction lead-free copper-based sliding bearing material and a preparation method thereof. The ferrous sulfide powder, the bismuth powder and the bronze powder are subjected to mechanical alloying by adopting a ball milling technology to improve the interface adhesive strength of the ferrous sulfide, the bismuth and the bronze, and the phenomenon that the ferrous sulfide is easy to agglomerate when the content of copper matrix is relatively high is improved, the structure of FeS is good in oil storage capacity, the stability of the liquid-solid lubricating film is enabled to be good, so that the process of Bi spalling, the fusion of the low-melting-point component Bi and separating out of the low-melting-point component Bi are relieved, and the liquid-solid lubricating film can also be repaired and completed, so that the antifriction performance of the material is improved; in conclusion, the antifriction and wear-resistant properties of the copper-basedsliding bearing material are improved, the lead which is used as a lubricant in the copper-based bearing material is replaced by the good synergistic effect of the ferrous sulfide and the bismuth, sothat the pollution of lead is avoided; and the antifriction lead-free copper-based sliding bearing material and the preparation method thereof have the advantages of being low in cost and suitable forindustrial production.
Owner:HEFEI UNIV OF TECH
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