Dental prosthesis and component thereof
a technology for dental prosthesis and components, applied in dental prosthesis, dental surgery, impression caps, etc., can solve problems such as infection and inflammation, and achieve the effect of preventing more effectively the invasion of germs
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preparation example 1
[0073]
[0074](Primary Particle Generating Step)
[0075]Dodecane [CH3(CH2)10CH3] was used as a continuous oil phase and pentaethylene glycol dodecyl ether [CH3(CH2)10CH2O(CH2CH2O)4CH2CH2OH] having a clouding point of 31° C. was used as a nonionic surfactant. At room temperature, 40 ml of the continuous oil phase containing 0.5 g of the nonionic surfactant was prepared. Next, 10 ml of 2.5 mol / l calcium hydroxide [Ca(OH)2] aqueous dispersion was added to the continuous oil phase prepared as above to prepare a water-in-oil type solution (W / O solution). While the W / O solution was stirred, 10 ml of 1.5 mol / l potassium dihydrogenphosphate [(KH2PO4)] solution was added thereto. Then, the solution was stirred at room temperature over 24 hours to cause a reaction. Next, the resulting reaction product was separated and washed by centrifugation to obtain a group of hydroxyapatite (HAp) primary particles.
[0076](Mixing Step)
[0077]1.0 g of a group of hydroxyapatite (HAp) primary particles was dispers...
preparation example 2
[0099]
[0100](Primary Particle Generating Step)
[0101]Dodecane [CH3(CH2)10CH3] was used as a continuous oil phase and pentaethylene glycol dodecyl ether [CH3(CH2)10CH2O(CH2CH2O)4CH2CH2OH] having a clouding point of 31° C. was used as a nonionic surfactant. At room temperature, 40 ml of the continuous oil phase containing 0.5 g of the nonionic surfactant was prepared. Next, 10 ml of 2.5 mol / l calcium hydroxide [Ca(OH)2] aqueous dispersion was added to the continuous oil phase prepared as above to prepare a water-in-oil type solution (W / O solution). While the W / O solution was stirred, 10 ml of 1.5 mol / l potassium dihydrogenphosphate [(KH2PO4)] solution was added thereto. Then, the solution was stirred at room temperature over 24 hours to cause a reaction. Next, the resulting reaction product was separated and washed by centrifugation to obtain a group of hydroxyapatite (HAp) primary particles.
[0102](Freezing / Thawing Step)
[0103]Thereafter, after a supernatant in a reaction vessel was tra...
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