Circularly polarizing plate and liquid crystal display
A liquid crystal display, circular polarizer technology, applied in polarizing elements, instruments, optics, etc., can solve problems such as low polarization performance, and achieve the effects of suppressing shrinkage, excellent polarization ability, and improving productivity
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Embodiment 1
[0372] [I] Preparation of λ / 4 Plates
[0373] 100g of 8-methyl-8-methoxycarbonyltetracyclo[4.4.0.12,5.17,10]dodec-3-ene, 60g of 1,2-dimethoxyethane, 240g of cyclohex Alkane and 3.4 ml of a 0.96 mol / l solution of diethylammonium chloride in toluene were added to an autoclave with an internal volume of 1 liter. Separately, 20 ml of a 0.05 mol / l solution of tungsten hexachloride in 1,2-dimethoxyethane and 10 ml of a 0.1 mol / l solution of paraldehyde in 1,2-dimethoxyethane Mix in a flask. 4.9 ml of this mixture was added to the mixture in the above autoclave. After the autoclave was sealed, the mixture was heated to 80°C with stirring for 3 hours. To the polymer solution thus obtained, a mixed solvent of 1,2-dimethoxyethane and cyclohexane (2 / 8 by weight) was added to adjust the polymer / solvent ratio to 1 / 10 (by weight) , and then 20 g of triethanolamine was added thereto and stirred for 10 minutes.
[0374] 500 g of methanol was added to the polymer solution, stirred for 30 ...
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