Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Method for producing lubricating oil base oil by hydrogenating tail oil

A technology for lubricating base oil and hydrogenated tail oil, which is applied in the fields of hydrotreating process, petroleum industry, and hydrocarbon oil treatment. The effect of simple process

Active Publication Date: 2008-08-27
CHINA PETROLEUM & CHEM CORP +1
View PDF10 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In summary, the existing technologies for producing lubricating oil base oils using hydrogenated tail oil as raw materials all need to carry out solvent dewaxing, catalytic dewaxing or isomerization dewaxing on the hydrogenated tail oil to achieve a lower pour point. purpose, the production process is more complicated

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Method for producing lubricating oil base oil by hydrogenating tail oil
  • Method for producing lubricating oil base oil by hydrogenating tail oil

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] 227.1 g of amorphous silica-alumina (SiO 2 The content is 45wt%, the pore volume is 0.75ml / g, and the specific surface area is 390m 2 / g), 18.8 grams of modified β molecular sieves, 65.8 grams of macroporous alumina (the pore volume is 1.0ml / g, and the specific surface area is 460m 2 / g) into the roller compactor, mixed for 30 minutes, then add 288.5 grams of binder (with a pore volume of 0.4ml / g and a specific surface area of ​​280m 2 / g of small-pore alumina 107.1g, HNO 3 Molar ratio to alumina is 0.3), rolling for 30 minutes, then add 60 ml of water, continue rolling until the paste can be extruded, extruded, and dried at 110°C for 6 hours. The dried strips were heated up to 580° C. and calcined for 4 hours to obtain the carrier. The carrier was impregnated with an impregnation solution containing tungsten and nickel for 2 hours at room temperature, dried at 120°C for 6 hours, and calcined at 480°C for 4 hours at programmed temperature to obtain a hydrotreating ca...

Embodiment 2

[0035] 252.8 grams of amorphous silicon aluminum (SiO 2 The content is 65wt%, the pore volume is 0.58ml / g, and the specific surface area is 340m 2 / g), 9.4 grams of modified β molecular sieves, 41.1 grams of macroporous alumina (pore volume is 0.75ml / g, specific surface area is 360m 2 / g) put into the roller compactor and mix for 20 minutes, then add 323.1 grams of binder (with a pore volume of 0.45ml / g and a specific surface area of ​​300m 2 / g small pore alumina 120.0g, HPO 3 The molar ratio to alumina is 0.2), continue rolling for 40 minutes, then add 55 ml of water, roll until the paste can be extruded, extrude, and dry the extruded strips at 140°C for 3 hours. The drying strip was heated to 530° C. and calcined for 5 hours to obtain the carrier. The carrier was impregnated with an impregnation solution containing tungsten and nickel at room temperature for 4 hours, dried at 130°C for 3 hours, and then calcined at 460°C for 5 hours to obtain catalyst B. The physical an...

Embodiment 3

[0038] 201.4 g of amorphous silica-alumina (SiO 2 The content is 30wt%, the pore volume is 0.89ml / g, and the specific surface area is 460m 2 / g), 31.3 grams of modified β molecular sieves, 82.8 grams of macroporous alumina (same as Example 1) were put into the roller compactor and mixed for 40 minutes, then added 265.4 grams of binding agent (same as Example 1), and continued Roll for 25 minutes, then add 30 milliliters of water, roll to extrude paste, extrude, and extrude at 130°C for 4 hours. The drying strip was heated up to 680° C. and calcined for 2.5 hours to obtain the carrier. The carrier was impregnated with an impregnation solution containing tungsten and nickel at room temperature for 8 hours, dried at 130°C for 4 hours, and calcined at 530°C for 3 hours to obtain catalyst C. The physical and chemical properties are shown in Table 1.

[0039] The properties of the modified β molecular sieve are: molecular sieve SiO 2 / Al 2 o 3 Weight ratio 85, specific surface...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
pour pointaaaaaaaaaa
specific surface areaaaaaaaaaaa
specific surface areaaaaaaaaaaa
Login to View More

Abstract

The present invention provides method of producing base oil for lubricant oil with hydrogenated tail oil. Hydrogenated tail oil as material is treated through one white clay refining process or one medium pressure hydrogenating and refining process under proper condition to obtain the lubricant oil base oil product. The hydrogenated tail oil is produced with vacuum gas oil, refined solvent oil or Fischer-Tropsch synthesized oil as material and through hydrocracking or hydrotreating process under the action of hydrogenating catalyst, and has pour point lower than -10 deg.c. The lubricant oil base oil product has excellent performance.

Description

technical field [0001] The invention relates to a method for producing lubricating oil base oil from hydrogenated tail oil. The hydrogenated tail oil obtained by treating with a hydrogenation catalyst with a strong isomerization function is selected for direct clay refining or medium-pressure hydrogenation supplementary refining to produce lubricating oil base. oil method. Background technique [0002] The traditional production of lubricating oil base oils adopts solvent refining process. The process of producing base oils with this solvent refining process has a history of nearly a century. The main two steps are still solvent refining to remove non-ideal components such as aromatics and Solvent dewaxing to ensure the cold flow properties of the base oil. In addition, white clay or hydrogenation supplementary refining is generally carried out. [0003] The increasingly stringent environmental regulations and the rapid development of the machinery industry have put forwar...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C10G67/06
Inventor 关明华全辉姚春雷刘平林振发
Owner CHINA PETROLEUM & CHEM CORP
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products