Process of producing oxygenated paraffin soap
A technology for oxidizing paraffin soap and a production method, which is applied in petrochemical modification, solid separation, flotation and other directions, can solve the problems affecting the content of main active ingredients of products, low active ingredients, long time, etc., and achieves acceleration of saponification reaction speed. , Increase the product yield, the effect of rapid stratification of soap liquid
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Embodiment 1
[0022] First put the raw wax and recovered wax into the preheating tank at a ratio of 6:4, remove impurities, separate water, dehydrate and heat up to 120°C for later use. The input amount of potassium salt and manganese salt is 1.6‰, and soda ash is input at 0.4‰ In the dissolving tank, add an appropriate amount of clear water and heat to dissolve for later use, take caustic soda with 50% material volume, and make an alkali solution with a concentration of 25% for later use;
[0023] Then put the preheated material in the preheating tank into the oxidation tower, and turn on the blower at the same time, supply air to the oxidation tower at an air volume of 40 cubic meters per ton per hour, and supply heat to the heating system in the tower in sufficient amount. Prepare the mixed solution of catalyst and soda ash and pour it into the tower. When the temperature of the material in the tower reaches 160±2°C, it will start to trigger, keep it for 0.5 hours, increase the air supply...
Embodiment 2
[0030] Pour the raw wax and recovered wax into the preheating tank at a ratio of 7:3, remove impurities, separate water, dehydrate and heat up to 120°C for later use. The dosage of potassium salt and manganese salt is 1.8‰, and soda ash is dissolved at 0.6‰ In the tank, add appropriate amount of clear water and heat to dissolve for later use, take caustic soda with 50% of the material volume, and make an alkali solution with a concentration of 28% for later use. The subsequent preparation, saponification, refining and packaging steps of oxidized wax are the same as in Example 1, the main quality indicators are the same as in Example 1, and the treatment of unsaponifiable matter is also the same as in Example 1.
Embodiment 3
[0032] Pour the raw wax and recovered wax into the preheating tank at a ratio of 8:2, remove impurities, separate water, dehydrate and heat up to 120°C for later use. The input amount of potassium salt and manganese salt is 2‰, and soda ash is dissolved at 0.8‰. In the tank, add an appropriate amount of clear water and heat to melt for later use, take caustic soda with a material volume of 50%, and make an alkali solution with a concentration of 30% for later use. The subsequent preparation, saponification, refining and packaging steps of oxidized wax are the same as in Example 1, the main quality indicators are the same as in Example 1, and the treatment of unsaponifiable matter is also the same as in Example 1.
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