High-brightness PDP red fluorescent material, and its preparing method
A red fluorescence, high-brightness technology, used in luminescent materials, chemical instruments and methods, etc., can solve the problems of poor color purity and affecting the color rendering range of the picture.
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Embodiment 1
[0034] Starting materials: yttrium oxide, europium oxide, bismuth oxide, boric acid
[0035] Raw materials are stoichiometrically ratio Y 0.9-x Bi x BO 3 :Eu 3+ (0≤x≤0.1) Accurately weighed, 10% of boric acid is excessive to supplement the loss of volatilization at high temperature. After grinding and mixing the raw materials evenly, first keep warm at 400-600°C for 2.5 hours, and then keep warm at 1000-1200°C for 3 hours hour, the product Y was obtained 0.9-x Bi x BO 3 :Eu3+ (0≤x≤0.1).
Embodiment 2
[0037] Starting materials: yttrium oxide, europium oxide, lanthanum oxide, boric acid
[0038] Raw materials are stoichiometrically ratio Y 0.9-x La x BO 3 :Eu 3+ (0≤x≤0.1) Accurately weighed, 10% of boric acid is excessive to supplement the loss of volatilization at high temperature. After grinding and mixing the raw materials evenly, first keep warm at 400-600°C for 2.5 hours, and then keep warm at 1000-1200°C for 3 hours hour, the product Y was obtained 0.9-x La x BO 3 :Eu 3+ (0≤x≤0.1).
Embodiment 3
[0040] Starting materials: yttrium oxide, europium oxide, scandium oxide, boric acid
[0041] Raw materials are stoichiometrically ratio Y 0.9-x sc x BO 3 :Eu 3+ (0≤x≤0.1) accurately weighed, wherein boric acid is over 10% to supplement the loss of volatilization at high temperature. After grinding and mixing the raw materials evenly, first keep warm at 400-600°C for 2.5 hours, and then keep warm at 1000-1200°C for 3 hours to obtain the product Y 0.9-x sc x BO 3 :Eu 3+ (0≤x≤0.1).
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