Making method for inorganic proton exchange film fuel cell film pole

A proton exchange membrane and fuel cell membrane technology, which is applied to fuel cell components, fuel cells, battery electrodes, etc., can solve the problem that the working temperature cannot exceed 200 °C, and achieve the effect of high heat dissipation efficiency.

Inactive Publication Date: 2007-09-12
WUHAN UNIV OF TECH
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Problems solved by technology

However, since polymers are used as proton-conducting materials in...

Method used

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  • Making method for inorganic proton exchange film fuel cell film pole

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Embodiment 1

[0038] Embodiment 1: As shown in Figure 1,

[0039] 1. The preparation of inorganic proton exchange membrane is carried out according to the following steps:

[0040] 1) Weigh 20.8 grams of HPW (phosphotungstic acid) and 41.6 grams of ethyl orthosilicate, dissolve them in a mixed solvent composed of 50 grams of water and 500 grams of ethanol, and stir them electromagnetically for 15 minutes to obtain phosphotungstic acid and ethyl orthosilicate mixed solution of esters.

[0041] 2) Weigh 14 grams of surfactant P123, dissolve it in a mixed solvent composed of 50 grams of water and 500 grams of ethanol, and stir it electromagnetically for 15 minutes to obtain a solution of surfactant P123.

[0042] 3) Slowly add the surfactant P123 solution prepared in step 2) to the mixed solution of phosphotungstic acid and ethyl orthosilicate prepared in step 1), and stir at room temperature for 1 hour to prepare an inorganic proton conductive powder precursor .

[0043] 4) Put the inorgan...

Embodiment 2

[0048] 1. The preparation of inorganic proton exchange membrane, process is carried out according to the following steps:

[0049] 1) Weigh 4 grams of HPMo (phosphomolybdic acid) and 8 grams of tetraethoxysilane, dissolve in a mixed solvent of 50 grams of water and 150 grams of ethanol, and stir electromagnetically for 20 minutes to obtain phosphomolybdic acid and tetraethoxysilane Silane mixed solution.

[0050] 2) Weigh 4 grams of surfactant PMAA, dissolve it in a mixed solvent composed of 50 grams of water and 150 grams of ethanol, and stir it electromagnetically for 20 minutes to obtain a solution of surfactant PMAA.

[0051] 3) The surfactant PMAA solution prepared in step 2) was slowly added to the mixed solution of phosphomolybdic acid and tetraethoxysilane prepared in step 1), and stirred at room temperature for 1 hour to prepare an inorganic proton conductive powder precursor.

[0052] 4) Put the inorganic proton conduction powder precursor prepared in step 3) in a p...

Embodiment 3

[0057] 1. The preparation of inorganic proton exchange membrane, process is carried out according to the following steps:

[0058] 1) Weigh 1 gram of HSiW (silicotungstic acid) and 10 grams of ethyl titanate, dissolve them in a mixed solvent consisting of 50 grams of water and 250 grams of ethanol, and stir them electromagnetically for 30 minutes to obtain a mixture of silicotungstic acid and ethyl titanate solution.

[0059] 2) Weigh 10 grams of surfactant PEG, dissolve it in a mixed solvent composed of 50 grams of water and 250 grams of ethanol, and stir it electromagnetically for 30 minutes to obtain a surfactant PEG solution.

[0060] 3) Slowly add the surfactant PEG solution prepared in step 2) into the mixed solution of silicotungstic acid and ethyl titanate prepared in step 1), and stir at room temperature for 2 hours to prepare an inorganic proton conductive powder precursor.

[0061]4) placing the inorganic proton-conducting powder precursor prepared in step 3) in a ...

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Abstract

The invention relates to an inorganic proton exchange membrane fuel cell membrane electrode preparation method. the preparation method, its characteristic lies in that it includes the following steps: 1) inorganic proton exchange membrane preparation: a) first prepares the heteropolyacid and the inorganic oxide compound forerunner body mix solution; b) the surface active agent solution preparation; c) inorganic proton conduction powder forerunner body preparation; d) inorganic proton exchange membrane preparation: The inorganic proton conduction powder forerunner body which step c) prepares sets in the culture dish, dry, high temperature burning, obtains the inorganic proton conduction powder, joins the thermoplastic resin cementing agent rmo-compression to prepare the inorganic proton exchange membrane; 2) inorganic proton exchange membrane-catalysis layer module preparation; 3) inorganic proton exchange membrane -catalysis layer module seal; 4) inorganic proton exchange membrane fuel cell membrane electrode preparation. The membrane electrode operating temperature of the method preparation is high (may be higher than 200 degree centigrade).

Description

technical field [0001] The invention relates to a preparation method of membrane electrodes of inorganic proton exchange membrane fuel cells. Background technique [0002] Hydrogen is a ubiquitous element in nature and is a renewable and clean energy source. Scientists believe that hydrogen energy will make up for and gradually replace the increasingly depleted fossil energy sources such as coal and oil in the 21st century, and become an important part of the world's energy pattern. Proton Exchange Membrane Fuel Cell (PEMFC) is an important way to convert hydrogen energy into electrical energy. Its energy conversion efficiency is as high as 50%, and it has low operating temperature and low noise. The only discharge is pure water. , which can be widely used in vehicle power sources and stationary power station power sources. Therefore, it is generally believed that fuel cells are the preferred clean and efficient power generation technology in the 21st century (Yi Baolian, ...

Claims

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Application Information

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IPC IPC(8): H01M8/02H01M4/88H01M2/14H01M8/1004
CPCY02E60/50Y02P70/50
Inventor 唐浩林潘牧
Owner WUHAN UNIV OF TECH
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