Nano bionic self-organization lubricating oil additive and preparation method thereof
A lubricating oil additive, bionic self-organization technology, applied in the direction of additives, lubricating compositions, petroleum industry, etc., can solve problems such as mechanical equipment corrosion, achieve the effect of wide application and better actual benefits
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Embodiment 1
[0058] Embodiment 1 nano-bionic vehicle lubricating oil additive
[0059] Select raw materials according to the following weight ratio:
[0060] 4'-(4"-n-alkoxyphenyleneethynyl) 4-n-hexyloxyazobenzene (azobenzene compounds) 1.0 parts
[0061] Triton-100 (as a phase transfer catalyst) 1.5 parts
[0062] Dodecyl petroleum sulfonic acid (as a microemulsifying surfactant) 4 parts
[0063] Glyceryl alcohol or n-heptanol (as a microemulsification aid) 6 parts
[0064] n-octylamine (as interface modifier) 2 parts
[0065] Add the azobenzene compound (4'-(4"-n-alkoxyphenyleneethynyl) 4-n-hexyloxyazobenzene) into the reaction kettle at 1.5 atmospheric pressure and 80°C temperature, Then add Triton-100, and continue to stir so that the temperature and pressure remain constant;
[0066] After stirring evenly, add dodecyl petroleum sulfonic acid, glycerol or n-heptanol and n-octylamine into the reactor;
[0067] The temperature was raised to 90° C., and the reaction kettle was kep...
Embodiment 2
[0069] Embodiment 2 Nano-bionic gear oil additive
[0070] Select raw materials according to the following weight ratio:
[0071] 1 part of octyloxyaminobiphenyl (as a self-organized molecule)
[0072] Tween 40 (as a phase transfer catalyst) 2 parts
[0073] Stearic acid (as a microemulsifying surfactant) 3.8 parts
[0074] Propylene glycol monoethyl ether (as a microemulsification aid) 5.8 parts
[0075] Octadecylamine (as interface modifier) 2 parts
[0076] The nano-bionic gear oil additive was prepared according to the method of Example 1, the difference being that: the reaction temperature was controlled at 85° C., and the reactor was reacted at 1 atmospheric pressure for 5 hours.
Embodiment 3
[0077] Embodiment 3 nano-bionic industrial grease additive
[0078] 1 part of octyloxyaminobiphenyl (as a biphenyl compound)
[0079] Spai 60 (as a phase transfer catalyst) 2.5 parts
[0080] Salicylic acid (as microemulsion surfactant) 3.7 parts
[0081] Octadecyl (triethoxy) silane (as a microemulsification aid) 6.2 parts
[0082] Heptyloxybenzoic acid (as interface modifier) 2 parts
[0083] The nano-bionic gear oil additive was prepared according to the method of Example 1, the difference being that: the reaction temperature was controlled at 85° C., and the reaction kettle was reacted for 4 hours at a pressure of 1 atmosphere.
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