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Industrial evaporator

An evaporation device, industrial technology, applied in the direction of evaporation, chemical instruments and methods, separation methods, etc., can solve the problems of retention, no reduction of distribution pipes, etc., and achieve the effect of small uneven molecular weight

Active Publication Date: 2007-11-28
ASAHI KASEI KK
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, since the high-viscosity material supplied from the high-viscosity material supply port (7) stays in the "dead space" between the porous plate (3) and the inner side wall surface of the hollow body for a long time, the above-mentioned problems inevitably arise.
In addition, even in the recently proposed patent document 8, there is no proposal at all to reduce the "dead space" in the distribution pipe 3 (Fig. 2) and the supply area (Fig. 3a) to the perforated plate.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0122] An industrial evaporation device with a disk-shaped flow path control member 20 and a guider 4 with a thickness of about 2 cm shown in Fig. 2 and Fig. 3 . The disk-shaped flow path control member 20 is hung and fixed from above at a distance of about 8 cm from the upper inner wall surface 23 of the liquid supply region 3 . In addition, the distance between the inner side wall surface 22 of the liquid supply region 3 and the flow path control member 20 is about 9 cm, and the distance between the porous plate 2 and the flow path control member 20 is about 8 cm. In addition, the peripheral portion of the disk-shaped flow path control member 20 is finished into a semicircle with a radius of about 1 cm in vertical section, and it is designed so that liquid does not stagnate in the peripheral portion. In addition, the cross-section of the connection portion between the inner side wall surface 23 of the liquid supply region and the perforated plate 2 is finished into a concave...

reference example 1

[0124] An aromatic polycarbonate was produced using the industrial evaporator of Example 1 as a polymerizer for condensation-based polymers. A molten prepolymer of aromatic polycarbonate (number-average molecular weight Mn: 4,000) produced from bisphenol A and diphenyl carbonate (the molar ratio relative to bisphenol A is 1.05) and maintained at 260°C is supplied by The pump supplies continuously from the supply port 1 into the supply area 3 . While flowing from the peripheral portion of the perforated plate 2 to the central portion, the molten prepolymer continuously supplied from the holes of the perforated plate to the evaporation region 5 (polymerization reaction region) proceeds polymerization reaction while flowing down the guide 4 . The polymerization reaction zone was maintained at 80 Pa through the vaporized product outlet 6 . The produced aromatic polycarbonate entering the polymerizer bottom 11 from the lower part of the guide 4 was continuously discharged from the...

Embodiment 2

[0128] Two sets of industrial evaporators shown in Figure 2 and Figure 3 with flow path control components 20 and guides are arranged in series to polymerize polycondensation polymers. The aromatic polycarbonate was produced using this polymerization facility (the first polymerizer and the second polymerizer). The materials of these evaporation devices are all stainless steel. The discharge pump 8 of each evaporator is a gear pump. The first polymerizer of the guider contact flow type has a cylindrical side shell 10 and a conical bottom shell 11, and L=950cm, h=850cm, D=400cm, d=20cm, C=150 degrees, S=750m 2 , A=12.56m 2 , A / B=400, D / d=20, L / D=2.375, r=0.3cm. The distance K between the guider closest to the inner wall of the evaporation area and the inner wall is about 14 cm. In addition, the diameter of the cross section of the flow path control member 20 is slightly smaller, but has the same shape as described in Embodiment 1, and the distance from the wall surfaces (23 ...

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Abstract

The problem to be solved by the present invention is to specifically disclose an industrial evaporating device, which makes the liquid containing a substance with a lower boiling point than the liquid flow down the outer surface of the guide, and evaporates the low-boiling substance during this process. The device can make the liquid evaporated and processed stably for a long time on an industrial scale of more than 1 ton per hour; further specifically discloses an industrial evaporation device that does not cause denaturation problems due to a part of the liquid staying for a long time. By providing an industrial evaporating device in which the guide itself has no heating source, and a flow path control member is provided in the liquid supply area, the flow path control member has a function to make the flow of the liquid supplied from the liquid receiving port to the porous plate mainly flow from the porous plate. The function of the peripheral part of the plate to flow in the direction of the central part, and the distance K (cm) between the guider and the inner wall surface closest to the inner wall surface of the side shell of the evaporation area satisfies the formula (6) and has the formula (1) To formula (5), or formula (1) to formula (11), or formula (1) to formula (14) specific structure of the industrial evaporation device, can solve the above problems, and easily obtain high-quality, high-purity Concentrated liquids, condensation polymers, thermoplastic polymers, thereby completing the present invention.

Description

technical field [0001] The present invention relates to a new industrial evaporation device. More specifically, it relates to a device for causing a liquid containing a substance having a lower boiling point than the liquid to flow downward along the outer surface of a guide which itself has no heating source, during which the substance having a lower boiling point is evaporated. Background technique [0002] Various devices are known as industrial evaporators for evaporating and removing volatile components and / or low boiling point components in a liquid and concentrating the liquid. For example, in the 6th edition of Handbook of Chemical Engineering (refer to Non-Patent Document 1: 6th Edition, Handbook of Chemical Engineering, pages 403-405, edited by the Society of Chemical Engineering, 1999), it is described that the submerged combustion method and the natural circulation type immersion tube Type, natural circulation horizontal tube type, vertical short tube type, vert...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D1/00C08G85/00
CPCC08G64/406B01D1/22C08G63/90B01D1/00C08G85/00
Inventor 福冈伸典八谷广志松崎一彦
Owner ASAHI KASEI KK
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