Industrial evaporator
An evaporation device, industrial technology, applied in the direction of evaporation, chemical instruments and methods, separation methods, etc., can solve the problems of retention, no reduction of distribution pipes, etc., and achieve the effect of small uneven molecular weight
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Embodiment 1
[0122] An industrial evaporation device with a disk-shaped flow path control member 20 and a guider 4 with a thickness of about 2 cm shown in Fig. 2 and Fig. 3 . The disk-shaped flow path control member 20 is hung and fixed from above at a distance of about 8 cm from the upper inner wall surface 23 of the liquid supply region 3 . In addition, the distance between the inner side wall surface 22 of the liquid supply region 3 and the flow path control member 20 is about 9 cm, and the distance between the porous plate 2 and the flow path control member 20 is about 8 cm. In addition, the peripheral portion of the disk-shaped flow path control member 20 is finished into a semicircle with a radius of about 1 cm in vertical section, and it is designed so that liquid does not stagnate in the peripheral portion. In addition, the cross-section of the connection portion between the inner side wall surface 23 of the liquid supply region and the perforated plate 2 is finished into a concave...
reference example 1
[0124] An aromatic polycarbonate was produced using the industrial evaporator of Example 1 as a polymerizer for condensation-based polymers. A molten prepolymer of aromatic polycarbonate (number-average molecular weight Mn: 4,000) produced from bisphenol A and diphenyl carbonate (the molar ratio relative to bisphenol A is 1.05) and maintained at 260°C is supplied by The pump supplies continuously from the supply port 1 into the supply area 3 . While flowing from the peripheral portion of the perforated plate 2 to the central portion, the molten prepolymer continuously supplied from the holes of the perforated plate to the evaporation region 5 (polymerization reaction region) proceeds polymerization reaction while flowing down the guide 4 . The polymerization reaction zone was maintained at 80 Pa through the vaporized product outlet 6 . The produced aromatic polycarbonate entering the polymerizer bottom 11 from the lower part of the guide 4 was continuously discharged from the...
Embodiment 2
[0128] Two sets of industrial evaporators shown in Figure 2 and Figure 3 with flow path control components 20 and guides are arranged in series to polymerize polycondensation polymers. The aromatic polycarbonate was produced using this polymerization facility (the first polymerizer and the second polymerizer). The materials of these evaporation devices are all stainless steel. The discharge pump 8 of each evaporator is a gear pump. The first polymerizer of the guider contact flow type has a cylindrical side shell 10 and a conical bottom shell 11, and L=950cm, h=850cm, D=400cm, d=20cm, C=150 degrees, S=750m 2 , A=12.56m 2 , A / B=400, D / d=20, L / D=2.375, r=0.3cm. The distance K between the guider closest to the inner wall of the evaporation area and the inner wall is about 14 cm. In addition, the diameter of the cross section of the flow path control member 20 is slightly smaller, but has the same shape as described in Embodiment 1, and the distance from the wall surfaces (23 ...
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Abstract
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