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System and process for continuous industrial preparation of 3-chloropropylchlorosilanes

A technology of allyl chloride and equipment, which is applied in the field of equipment and methods for continuous industrial preparation of 3-chloropropylchlorosilane, and can solve the problems of lacking and unrealized organosilane micro-reactor technology, etc.

Inactive Publication Date: 2008-03-12
GOLDSCHMIDT CHEM CORP
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, microreactor technology for the industrial production of organosilanes is still lacking or at least not realized

Method used

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  • System and process for continuous industrial preparation of 3-chloropropylchlorosilanes
  • System and process for continuous industrial preparation of 3-chloropropylchlorosilanes
  • System and process for continuous industrial preparation of 3-chloropropylchlorosilanes

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Embodiment

[0080] Preparation of 3-Chloropropyltrichlorosilane

[0081] The equipment used for the preparation of chloropropyltrichlorosilane is mainly composed of educt storage, diaphragm pump, adjustment assembly, measurement assembly and metering assembly, a T-mixer, 2 series replaceable and equipped with packing (average diameter of 1.5mm stainless steel ball), a prereactor (diameter 5cm, length 40mm, stainless steel), a stainless steel capillary (diameter 1mm, length 50m), a constant temperature bath for prereactor and capillary temperature regulation, a pressure stabilization valve, a continuous N2 Operation of the stripping column, and piping required for input of educts and output of products, recycle and waste gases.

[0082] First at room temperature olefin (propenyl chloride) and platinum-catalyst [53 g hexachloroplatinic acid-hexahydrate in 1 L acetone] were metered in molar ratio olefin:Pt=200000:1, mixed, and In the mixer, it is mixed with trichlorosilane (TCS, Degussa Com...

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Abstract

The present invention relates to an equipment, a reactor and a method for the reaction in the continuous industry, wherein the allyl chloride A reacts with the His-compound B at the condition that the catalyst C and the random additional accessory material exist, the equipment at least is based on an educt jointing apparatus (3) of the component A(1) and B(2), at least one multicomponent reactor (5) and a product after-treating device (8), the multicomponent reactor (5) includes at least two reactor component which is the form of replaceable pre-reactor (5.1) and at least one else reactor component (5.3) at the downriver side of the pre-reacting system.

Description

technical field [0001] The present invention relates to a new reactor and plant for the continuous industrial preparation of 3-chloropropylchlorosilanes by reacting allyl chloride with HSi-compounds and the process involved. Background technique [0002] Organosilanes, such as vinylchlorosilanes or vinylalkoxysilanes (EP 0456 901A1, EP 0 806427 A2), chlorinated alkylchlorosilanes (DE-AS 28 15 316, EP 0 519 181 A1, DE 195 34 853A1 , EP 0 823 434 A1, EP 1 020 473 A2), alkylalkoxysilanes (EP 0 714 901 A1, DE 101 52 284 A1), fluorinated alkylalkoxysilanes (EP 0 838 467 A1, DE 103 01 997 A1), aminoalkylalkoxysilanes (DE-OS 27 53 124, EP 0 709 391 A2, EP 0 849 271 A2, EP1 209162 A2, EP 1 295 889 A2), glycidyloxyalkyl Alkoxysilanes (EP 1 070 721 A2, EP 0 934 947 A2), Methacrylateoxyalkylalkoxysilanes (EP 0 707 009 A1, EP 0 708 081A2), Polyetheralkylalkoxysilanes (EP 0 387 689 A2) and others etc., there are high-tech industrial needs. Methods and equipment for their production ha...

Claims

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Application Information

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IPC IPC(8): C07F7/12C07F7/14
Inventor J·E·朗G·马科维茨D·维沃斯H·梅茨N·施拉德贝克
Owner GOLDSCHMIDT CHEM CORP
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