Carbon dioxide acceptors
A technology of carbon dioxide and acceptors, applied in zirconia, inorganic chemistry, carbon compounds, etc., can solve problems such as sintering
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Embodiment 1
[0089] SolA: 100 g of zirconyl nitrate hydrate dissolved in 1 liter of deionized water.
[0090] SolB: 100 g of lithium acetate dihydrate dissolved in 1 liter of deionized water.
[0091] The mixture was stirred overnight and stored in a sealed bottle.
Embodiment 2
[0093] The solution prepared in Example 1 was standardized by thermogravimetric analysis in order to calculate the ZrO per g of solution that can be obtained by its calcination 2 and Li 2 The amount of O. For this purpose, known quantities of each solution were placed in pre-dried alumina crucibles. The samples were calcined and the weight of the resulting oxide was measured. The alumina crucible was dried and calcined in a muffle furnace at 1000° C. for 12 hours. The heating and cooling rate was 200°C / h. The result obtained is: 3.03×10 -4 mol ZrO 2 / g solA and 5.02×10 -4 mol Li 2 O / g solB.
Embodiment 3
[0095] Mix appropriate amounts of solA and solB prepared in Example 1 to synthesize 10 g of Li 2 ZrO 3 (0.065 mol). According to the standardized results in Example 2, 215 g of solA (0.065 mol of ZrO 2 ) and 130g of solB (0.065mol of Li 2 O) Mix and stir overnight.
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