Emulsion for vibration damper
A vibration damping material and emulsion technology, which is applied in non-rotational vibration suppression, other chemical processes, coatings, etc., can solve problems such as cracks on the surface of the coating film and insufficient film formation
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Embodiment 1
[0135] Deionized water (76 parts) was added to a polymerizer equipped with a stirrer, reflux condenser, thermometer, nitrogen gas inlet and dropping funnel. Then, the internal temperature was raised to 70° C. with stirring under nitrogen flow. On the other hand, in the dropping funnel, add monomer emulsion 1, this monomer emulsion 1 is made of methyl methacrylate (54.4 parts), acrylate-2-ethylhexyl (44.6 parts), acrylic acid (1.0 parts), tert-dodecyl mercaptan (0.4 parts), sulfate ester salt of polyoxyethylene alkyl ether (manufactured by Daiichi Kogyo Pharmaceutical Co., Ltd., "Hitenol NF-08", 15 parts) adjusted to a 20% aqueous solution beforehand, and deionized water (10 servings) made up.
[0136] Add monomer emulsion 1 dropwise to a polymerizer whose temperature is adjusted to 70°C to start the reaction, and after raising the temperature to 80°C, uniformly drop monomer emulsion 1 over 2 hours while maintaining the internal temperature at 80°C . Simultaneously, 5% potas...
Embodiment 2~16
[0142] An emulsion for a vibration damping material was obtained in the same manner as in Example 1 except that the composition of the monomer components for forming the core portion and the shell portion was adjusted to the compositions shown in Table 1 and Table 2.
[0143] Various physical properties and the like were evaluated for this emulsion for vibration damping material in the same manner as in Example 1. The results are listed in Table 1 and Table 2. In addition, the areal weight of Example 11 on the substrate was determined. The results are listed in Table 5.
Embodiment 17
[0145] The composition of the monomer components used to form the core and the shell was adjusted to the composition shown in Table 2, and 1.5 parts of foaming agent ("EXPANCEL WU642 ", Japanese Fillite company manufactures), except that is identical with embodiment 1, obtains the emulsion for damping material.
[0146] Various physical properties and the like were evaluated for this emulsion for vibration damping material in the same manner as in Example 1. The results are listed in Table 2.
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