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80results about How to "Less additives" patented technology

Graphene grinding and stripping device, graphene production system and production method

ActiveCN104401971AKeep the natural plane sizeReduce the chance of crushingCvd grapheneMechanical engineering
The invention discloses a graphene grinding and stripping device which comprises an upper grinding disc, a lower grinding disc, a driving mechanism for driving the upper grinding disc to rotate, and a material collection mechanism for collecting a product after grinding, wherein the upper grinding disc and the lower grinding disc are matched with each other; a horizontal contact surface is formed between the upper grinding disc and the lower grinding disc, the upper grinding disc is provided with an upper feed inlet, the lower grinding disc is provided with a lower feed inlet, the upper feed inlet and the lower feed inlet are both connected with the contact surface between the upper grinding disc and the lower grinding disc, and the lower end of the lower feed inlet is in sealed connection with one water inlet tube; moreover, the upper end face of the lower grinding disc is provided with a groove, and an annular region formed by rotary surrounding of the lower end of the upper feed inlet is surrounded in the groove. The graphene grinding and stripping device can realize large-size successful stripping of graphene. The invention also relates to a graphene production system containing the graphene grinding and stripping device and a graphene production method.
Owner:江苏碳谷二维世界科技有限公司

Rotary graphene stripping device, graphene production system and production method

ActiveCN104401970AReduced chance of crushingKeep the natural plane sizeGraphiteEngineering
The invention discloses a rotary graphene stripping device including a rotary cylinder body; a top cover is arranged above the rotary cylinder body, a bottom cover is arranged below the rotary cylinder body, the top of the top cover is provided with a feed inlet, the bottom of the bottom cover is provided with a discharge port, and the feed inlet is communicated with the interior of the rotary cylinder body; the outer side of the rotary cylinder body is provided with a first motor, and is used for driving the rotary cylinder body to horizontally rotate; the rotary cylinder body is also internally provided with an inner cylinder, and a second motor used for driving the inner cylinder to horizontally rotate in a direction opposite to the rotating direction of the rotary cylinder body is arranged below the rotary cylinder body; the upper part of the inner cylinder is shrunk in a certain angle, and a material storage space is left between the upper part of the inner cylinder and the upper part of the rotary cylinder body; the lower part of the inner cylinder and the lower part of the rotary cylinder body are in clearance fit to be used for grinding graphite sheets, and a clearance between the lower part of the inner cylinder and the lower part of the rotary cylinder body is successively decreased downward along the axial direction of the rotary cylinder body. The rotary graphene stripping device can achieve successful stripping of graphene. The invention also relates to a graphene production system containing the rotary graphene stripping device and a graphene production method.
Owner:江苏碳谷二维世界科技有限公司

Polyether sulfone ultrafiltration membrane preparation method capable of improving permeability and selectivity simultaneously

The invention discloses a polyether sulfone ultrafiltration membrane preparation method capable of improving permeability and selectivity simultaneously. An ultrafiltration membrane is prepared by adopting a phase inversion method, and PEI (polyetherimide) is used as an additive, and is added to change the phase inversion process and regulate the structure of the PES ultrafiltration membrane to achieve high permeability and high selectivity. The preparation method comprises the following steps of (1) dissolving the PEI in a solvent (DMF) (dimethyl formamide), adding polyether sulfone and PVP (polyvinylpyrrolidone), and performing heating to dissolve the polyether sulfone and the PVP to form a homogeneous membrane coating solution; and (2) controlling membrane forming conditions, and preparing the flat membrane. According to the method, the structure of the PES ultrafiltration membrane is effectively regulated, and the aperture ratio of the PES ultrafiltration membrane and the thickness of a selective layer are increased to greatly improve the permeability and the selectivity; the preparation method is simple and suitable for being used in the industrial production and the preparation of a basic membrane of a nanofiltration membrane.
Owner:NANJING UNIV OF SCI & TECH

Device for continuously preparing graphene and method for producing graphene

The invention belongs to the technical field of graphene and particularly relates to a device for continuously preparing graphene and a method for producing graphene. The device comprises a raw material grinding tank, a grinding medium storage bin, a stirring tank, a continuous grinding mechanism, a material storage tank, a centrifugal filtering device and a drying device. A blade type stirring mill is arranged in the raw material grinding tank. The continuous grinding mechanism comprises a high-pressure pump, the grinding bin, a flow guide ring, a dispersion impeller and a transmission shaft. The flow guide ring is located in the middle of the grinding bin and fixedly connected with the transmission shaft, the dispersion impeller is located between the flow guide ring and the bottom of the grinding bin, and the transmission shaft passes through the center of the dispersion impeller. The probability that graphene is smashed is reduced through continuous stripping step by step, structural defects of graphene are reduced, and meanwhile the situation that structural defects are caused again to stripped graphene due to re-grinding is avoided. The invention further discloses the method for producing graphene by means of the device for continuously preparing graphene from the slurry.
Owner:淮安双洋新材料有限公司

Drinking type normal-temperature yoghourt and preparation method thereof

InactiveCN112616921AOvercoming problems with using multiple stabilizersAdd lessMilk preparationBiotechnologySucrose
The invention discloses drinking type normal-temperature yoghourt and a preparation method thereof. The drinking type normal-temperature yoghourt comprises the following raw materials: concentrated milk, cane sugar, milk protein powder, pectin, a thickening agent, a leavening agent and water. The preparation method comprises the following steps of: concentrating raw milk through a Reverse Osmosis (RO) membrane to obtain the concentrated milk; sterilizing and cooling the concentrated milk, and adding the milk protein powder and part of cane sugar to obtain a mixed base material; homogenizing and sterilizing the mixed base material, and cooling to a fermentation temperature to obtain a fermentation substrate; adding the leavening agent into the fermentation substrate for fermentation to obtain a yoghourt base material; heating water obtained by intercepting the Reverse Osmosis (RO) membrane, and adding the pectin, the thickening agent and the rest of cane sugar to obtain a mixed solution; performing high-speed shearing and stirring treatment, sterilizing and cooling to obtain a pectin solution; and mixing and stirring the obtained yoghourt base material and the obtained pectin solution in proportion to obtain a drinking type normal-temperature yoghourt base material, and homogenizing, sterilizing, cooling and filling the drinking type normal-temperature yoghourt base material to obtain the drinking type normal-temperature yoghourt. The drinking type normal-temperature yoghourt has the advantages that the protein content of the normal-temperature drinking type yoghourt is increased, the quantity of a stabilizer is reduced, and the drinking type normal-temperature yoghourt tastes fresh and cool.
Owner:BRIGHT DAIRY & FOOD

Method for separating arsenic and further recycling antimony and tin with copper anode slime reduction-organic vulcanization method

The invention relates to a method for separating arsenic and further recycling antimony and tin with a copper anode slime reduction-organic vulcanization method, and belongs to the technical field ofresource comprehensive recovery, utilization and environmental protection. The method includes the steps that copper anode slime and a reducing agent are evenly mixed after being ground at first, andreduction roasting volatilization arsenic removing is conducted under the inert gas shielding condition to obtain arsenic-containing soot and a first section of substrate; the obtained first section of the substrate and the reducing agent are evenly mixed after being ground, and reduction roasting is performed under the inert gas shielding condition to obtain the volatile product of antimony oxideand a second section of substrate; and the obtained second section of the substrate and an organic vulcanizing agent are evenly mixed after being ground, and reduction roasting is conducted under theinert gas shielding condition to obtain tin sulfide and a third section of substrate. The main phases of arsenic, antimony and tin in anode slime include As2O5, Cu3(AsO4)2, Sb2O4 and SnO2. By adoption of the method, the characteristics that high-value arsenic and antimony can be reduced easily and the oxide of the arsenic and antimony has different volatilities are fully utilized, and the arsenicand antimony separation problem of the copper anode slime is solved; and meanwhile the characteristics that the tin can be vulcanized easily and tin sulfide can volatilize easily are used for volatile recycling of the tin in the substrate.
Owner:ZHAOQING FEINAN METAL

Dyeing pretreatment process for cotton and cheese or warp beam containing cotton fiber

The invention provides a dyeing pretreatment process for cotton and cheese or warp beams containing cotton fiber, which is characterized by adopting the following steps: (1) treating the cheese or warp beams in a main cylinder by use of biological enzyme for 30 to 50 minutes at the temperature of between 40 and 55 DEG C, and bleaching the cheese or warp beams with oxygen for 30 to 50 minutes at the temperature of between 70 and 95 DEG C; (2) discharging water; (3) washing, discharging water again; and (4) performing enzyme treatment for removing hydrogen peroxide. As the process changes the prior pretreatment for the cotton and cheese or warp beams containing cotton fiber into biological enzyme treatment and oxygen bleaching and reduces the amount of caustic soda and hydrogen peroxide as auxiliaries, the process has the advantages that the maximum temperature of the process is 15 to 40 DEG C lower than of the temperature of the normal oxygen bleaching, the process reduces energy consumption, improves dye-uptake rate, reduces pollution on environment, allows pretreatment to be more friendly to environment, ensures that the whiteness and capillary effect after treatment are equivalent to that of the normal high-temperature pretreatment, improves the dye-uptake rate of cotton fiber, does not limit or affect dyeing process, does not need to replace equipment, has low energy consumption, and is simple to realize.
Owner:LUTAI TEXTILE

Method for preparing enzyme from kudzuvine roots and mulberry fruits

The invention discloses a method for preparing an enzyme from kudzuvine roots and mulberry fruits. The method comprises the following steps that the kuzuvine roots and the mulberry fruits are smashed by a pulping machine and mixed to be uniform; a mixture is poured into a fermentation container, a precooled disodium hydrogen phosphate-citric acid buffer solution is added, a complex enzyme and ferrous carbonate are added, and enzymatic low-temperature extraction is conducted; filtrate is extracted to prepare first-time fermentation liquor, the first-time fermentation liquor is inoculated with lactobacillus plantarum to prepare second-time fermentation liquor, and the second-time fermentation liquor is subjected to solid-liquid separation to obtain the enzyme. According to the method, through enzymatic low-temperature extraction, the nutritional ingredients in the kudzuvine roots and the mulberry fruits can be fully extracted, the product effect and edible safety are greatly improved, the technology is simple, and the prepared enzyme fully retains the effective ingredients of the kudzuvine roots and leaves and the mulberry fruits, is stable in quality, has multiple effects of reducing blood vessel resistance, improving cardio-cerebral blood circulation, reducing the myocardial oxygen consumption and the like and can achieve the nutrition and health care effects.
Owner:JIANSU MAOBAO GEYE CO LTD

Method for preparing ceramic micro-spheres of thorium oxide

The invention relates to a method for preparing ceramic micro-spheres of thorium oxide. The method includes dropwise adding ammonia water into thorium nitrate solution to form hydrolysis solution, dropwise adding glacial acetic acid into the hydrolysis solution to regulate the pH (potential of hydrogen) of the hydrolysis solution, and adding polyvinyl alcohol into the hydrolysis solution under stirring conditions to form thorium oxide colloidal solution; dispersing the thorium oxide colloidal solution to obtain liquid drop and allowing the liquid drop to sequentially flow through helium zones, ammonia gas zones and ammonia water zones; arranging dispersed gel particles in strong ammonia water and aging the dispersed gel particles; adding the aged gel particles and deionized water into a hydrothermal reaction kettle and carrying out temperature reaction; placing gel particles into a drying furnace after hydrothermal reaction is carried out on the gel particles, and heating and drying the gel particles under humidity control to form dried gel particles; placing the dried gel particles in a calcination furnace, filling the calcination furnace with air and heating and calcining the gel particles to obtain calcined gel particles; placing the calcined gel particles in a sintering furnace, filling the sintering furnace with air and heating and sintering the calcined gel particles to obtain the ceramic micro-spheres. The method has the advantage that the ceramic micro-spheres of the thorium oxide can be prepared by the aid of simple technologies.
Owner:SHANGHAI INST OF APPLIED PHYSICS - CHINESE ACAD OF SCI

A kind of vortex type graphene stripping device, graphene production system and production method

A vortex graphene stripping device is disclosed. The vortex graphene stripping device comprises an outer cylinder provided with a heating jacket. The outer cylinder is provided with a pressure gage for detecting the pressure in the outer cylinder and a temperature measuring device for measuring the temperature in the outer cylinder. The top of the outer cylinder is provided with a feed port. The middle and lower part of the outer cylinder is provided with a discharging port. An inner sleeve of the outer cylinder is provided with a truncated cone-shaped inner cylinder with a downward taper angle. The upper and lower ends of the inner cylinder are open. The inner cylinder is fixed in the outer cylinder in a suspension manner through a hollowed-out support. Shear blades used for stripping graphene flakes are tightly arranged on the inner wall of the inner cylinder. A groove is formed between each adjacent shear blades. A turbine is disposed between the lower end of the inner cylinder and the lower end of the outer cylinder, and is driven to rotate by a driving mechanism disposed outside the outer cylinder. Turbine blades are perpendicular to and towards the opening at the lower end of the inner cylinder. The vortex graphene stripping device can achieve successful stripping of graphene. The invention also relates to a graphene producing system comprising the vortex graphene stripping device and a graphene producing method.
Owner:江苏碳谷二维世界科技有限公司
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