The invention relates to the technical field of high-purity
manganese preparation, and discloses a high-purity
manganese preparation method using high and
low vacuum, which comprises the following steps: S0, pretreatment operation: before
pickling operation, carrying out mechanical
polishing or
sand blasting treatment on a
manganese sheet to remove oxides and
impurity layers on the surface; the method comprises the following steps: S1,
pickling operation: carrying out
pickling on a manganese sheet with the purity of 2N by using 0.5-10% dilute
sulfuric acid under an ultrasonic condition through cleaning equipment; s2, washing and
drying: washing the manganese sheet subjected to
acid washing in the step S1 with pure water through cleaning equipment under an ultrasonic condition, and transferring the manganese sheet into a
vacuum drying oven for
drying after the pure
water washing is completed; and S3, high-vacuum
smelting is conducted, specifically, manganese sheets obtained through washing and
drying in the step S2 are loaded into a suspension
smelting furnace,
smelting is conducted under the high-vacuum condition, high-purity
hydrogen is introduced, the manganese solution is subjected to
hydrogen treatment, and oxides and hydrides which are difficult to volatilize are removed. High-purity
hydrogen is introduced for treatment under a high-vacuum condition, and a low-vacuum pulling technology is combined, so that impurities are effectively removed, and the purity of a finished product is improved.