Horizontal type agitated bed reactor material volume detection method
The technology of a horizontal agitated bed and a detection method is applied to the detection of the material holding capacity of the horizontal agitated bed reactor and the detection of the material level of the solid particles in the polymerization kettle, and can solve the change of reading, false report of material level, no material level, etc. problems, to achieve the effect of low measurement conditions, easy and convenient installation, and small measurement errors
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Embodiment 1
[0042] use as figure 1 In the cold mold device shown, the horizontal reactor has a length of 1530mm and an inner diameter of 475mm, and is made of transparent plexiglass. The stirring paddle is blade-type, made of stainless steel, and the rotation speed is 15rpm. The acoustic emission signal is measured with an acoustic wave measuring instrument. The sound wave measuring instrument includes a sound wave receiving device, an amplifying device, a signal collecting device and a signal processing device, the sampling frequency is 500kHz, and the sampling time is 10s. The powder used in the experiment is impact polypropylene (a certain industrial device powder), and its melt index and density are 2.0g / 10min and 900kg / m3 respectively 3 , the average particle size is 312mm, and the particle size distribution is shown in Table 1.
[0043] Table 1. Particle Size Distribution of Impact Polypropylene
[0044]
[0045] Select the outer wall of the middle part of the horizontal react...
Embodiment 2
[0047] The detection of the material level in an industrial horizontal stirring polymerization reactor was carried out by using the acoustic wave measurement technology. The device is composed of two horizontal reactors connected in series, using BP-Amoco's patented product - Amoco CD catalyst, polymerized in a gas-phase horizontal tank close to plug flow, and can produce homopolymers (HP) and random copolymers (RCP), impact copolymer (ICP) and other products. The horizontal reactor is 13700mm in length, 2743mm in inner diameter, made of stainless steel, and the speed is maintained at 15r / min. Acoustic emission signals are measured by acoustic wave measuring instruments, which include acoustic wave receiving devices, amplification devices, signal acquisition devices and signal processing devices, with a sampling frequency of 1MHz and a sampling time of 5s. Remove a circle of insulation layer on the reactor insulation layer in advance, so that the acoustic emission sensor is d...
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