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On-line control multi-still continuous production method for wood adhesive

A wood adhesive and production method technology, applied in the direction of adhesive, simultaneous control of multiple variables, program control, etc., can solve problems such as poor stability, difficult chemical reaction and production process control, complex reaction history and production process, etc. Stable quality effect

Inactive Publication Date: 2011-08-31
GUANGXI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The control of the reaction end point is realized by adjusting the pH value and lowering the reaction temperature, so the reaction process and production process are more complicated
The production of wood adhesives at home and abroad usually adopts a single-pot batch method of production, and the control of chemical reactions and production processes is relatively difficult; especially in my country, process parameters and technical indicators are usually controlled manually, mostly by Manual sampling is used to detect the viscosity to judge the reaction end point. Manual sampling detection often lags behind the real reaction process, and the detection results are easily affected by human factors, which greatly affect the product quality.
On the whole, the quality stability of wood adhesive products is poor, and its output needs to be further improved

Method used

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  • On-line control multi-still continuous production method for wood adhesive
  • On-line control multi-still continuous production method for wood adhesive
  • On-line control multi-still continuous production method for wood adhesive

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Prepare urea-formaldehyde resin glue with the continuous production method of on-line control three kettle combination:

[0024] 1. The ratio of urea to formaldehyde is 1 (mol): 1.06 (mol); urea is added in three times, and formaldehyde is added once; the reaction kettle is 6 tons, the amount of formaldehyde: 3050 kg (mass fraction 36.6%), the amount of urea: 2150 kg (purity 98%).

[0025] 2. Start the computer monitoring and feedback system, collect temperature, PH value, viscosity and other data and import them into the PLC machine, then input them into the computer and start timing. In the first reactor, use the machine control system to open the solenoid valve to add the full amount of formaldehyde, then open the solenoid valve and use 30% caustic soda solution to automatically adjust the pH value to 8.0, then open the material solenoid valve to add the first metered urea ( Accounting for 52% of the total amount of urea), open the solenoid valve of the return syste...

Embodiment 2

[0031]Prepare urea-formaldehyde resin glue with the continuous production method of on-line control three kettle combination:

[0032] 1. The ratio of urea to formaldehyde is 1 (mol): 1.4 (mol); urea is added in four times, and formaldehyde is added in two times; the reaction kettle is 6 tons, the amount of formaldehyde: 3370 kg (mass fraction 36.6%), urea Dosage: 1800 kg (purity 98%).

[0033] 2. Start the computer monitoring and feedback system, collect temperature, PH value, viscosity and other data and import them into the PLC machine, then input them into the computer and start timing. In the first reactor, open the solenoid valve with the machine control system to add 80% of the total amount of formaldehyde, then open the solenoid valve and use 40% caustic soda solution to automatically adjust the pH value to 8.5, then open the material solenoid valve to add the first metering For secondary urea (accounting for 45% of the total urea), use the machine control system to o...

Embodiment 3

[0039] Prepare phenolic resin glue with the continuous production method of on-line control two kettle combinations:

[0040] Because the formulation of many wood adhesives does not require vacuum dehydration, the second reactor and the third reactor can be combined into one reactor according to the production process and equipment investment requirements, and the polycondensation reaction and the cooling stage are combined. for one.

[0041] 1. The ratio of phenol to formaldehyde is 1 (mol): 1.5 (mol); phenol is added once, and formaldehyde is added in two times; the reactor is 6 tons, and the amount of formaldehyde: 1970 kg (mass fraction 36.6%), the amount of phenol: 1530 kilograms (purity 98%), caustic lye consumption: 480 kilograms (mass fraction 40%), water consumption: 500 kilograms.

[0042] 2. Start the computer monitoring and feedback system, collect temperature, PH value, viscosity and other data and import them into the PLC machine, then input them into the comput...

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Abstract

The invention discloses an on-line control multi-kettle continuous type production method for wood adhesive. Complicated chemical reaction processes are decomposed in different reaction kettles, which simplifies the chemical reaction so that a computer control system of a computer operates and controls; the computer system is used to make on-line display, data processing, information feedback andautomatic control to processing parameters and technical targets such as reaction time, reaction temperature, pH values, viscosity and so on of each reaction kettle and each chemical reaction phase to achieve the aim of instant control of the magnitude of the average molecular weight, particularly the distribution of the magnitude of the molecular weight, of wood adhesive. The method of the invention can be used to produce a plurality of resin adhesive; the chemical reaction, the control principle and the actual operation of the materials are basically same as long as the technical targets such as processing parameters, production flow, pH values, and viscosity and so on are determined according to the concrete formula requirement.

Description

technical field [0001] The invention relates to the field of wood adhesive manufacture, in particular to a method for using a computer to automatically control the combination of multiple reaction kettles on-line to form a continuous production method. Background technique [0002] The production and preparation of wood adhesives basically go through two chemical reaction processes: addition reaction and polycondensation reaction. The production process generally goes through the stages of temperature rise, heat preservation, and temperature drop. During the production process, the viscosity is constantly increasing and the pH value is constantly changing. The control of the reaction end point is realized by adjusting the pH value and lowering the reaction temperature, so the reaction process and production process are relatively complicated. However, the production of wood adhesives at home and abroad usually adopts a single-pot batch method of production, and the control o...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G05D27/02G05B19/048C09J161/24
Inventor 甘卫星罗建举唐贤明赖炼苏初旺李宁
Owner GUANGXI UNIV