On-line control multi-still continuous production method for wood adhesive
A wood adhesive and production method technology, applied in the direction of adhesive, simultaneous control of multiple variables, program control, etc., can solve problems such as poor stability, difficult chemical reaction and production process control, complex reaction history and production process, etc. Stable quality effect
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Embodiment 1
[0023] Prepare urea-formaldehyde resin glue with the continuous production method of on-line control three kettle combination:
[0024] 1. The ratio of urea to formaldehyde is 1 (mol): 1.06 (mol); urea is added in three times, and formaldehyde is added once; the reaction kettle is 6 tons, the amount of formaldehyde: 3050 kg (mass fraction 36.6%), the amount of urea: 2150 kg (purity 98%).
[0025] 2. Start the computer monitoring and feedback system, collect temperature, PH value, viscosity and other data and import them into the PLC machine, then input them into the computer and start timing. In the first reactor, use the machine control system to open the solenoid valve to add the full amount of formaldehyde, then open the solenoid valve and use 30% caustic soda solution to automatically adjust the pH value to 8.0, then open the material solenoid valve to add the first metered urea ( Accounting for 52% of the total amount of urea), open the solenoid valve of the return syste...
Embodiment 2
[0031]Prepare urea-formaldehyde resin glue with the continuous production method of on-line control three kettle combination:
[0032] 1. The ratio of urea to formaldehyde is 1 (mol): 1.4 (mol); urea is added in four times, and formaldehyde is added in two times; the reaction kettle is 6 tons, the amount of formaldehyde: 3370 kg (mass fraction 36.6%), urea Dosage: 1800 kg (purity 98%).
[0033] 2. Start the computer monitoring and feedback system, collect temperature, PH value, viscosity and other data and import them into the PLC machine, then input them into the computer and start timing. In the first reactor, open the solenoid valve with the machine control system to add 80% of the total amount of formaldehyde, then open the solenoid valve and use 40% caustic soda solution to automatically adjust the pH value to 8.5, then open the material solenoid valve to add the first metering For secondary urea (accounting for 45% of the total urea), use the machine control system to o...
Embodiment 3
[0039] Prepare phenolic resin glue with the continuous production method of on-line control two kettle combinations:
[0040] Because the formulation of many wood adhesives does not require vacuum dehydration, the second reactor and the third reactor can be combined into one reactor according to the production process and equipment investment requirements, and the polycondensation reaction and the cooling stage are combined. for one.
[0041] 1. The ratio of phenol to formaldehyde is 1 (mol): 1.5 (mol); phenol is added once, and formaldehyde is added in two times; the reactor is 6 tons, and the amount of formaldehyde: 1970 kg (mass fraction 36.6%), the amount of phenol: 1530 kilograms (purity 98%), caustic lye consumption: 480 kilograms (mass fraction 40%), water consumption: 500 kilograms.
[0042] 2. Start the computer monitoring and feedback system, collect temperature, PH value, viscosity and other data and import them into the PLC machine, then input them into the comput...
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