Photosensitive composition, photosensitive film, photosensitive laminate, method of forming permanent pattern and printed board
A photosensitive composition, photosensitive layer technology, applied in the direction of printed circuit, printed circuit manufacturing, multilayer circuit manufacturing, etc.
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[0727] The present invention will be described more specifically through examples below, but the present invention is not limited thereto.
Synthetic example 1
[0729] 159 g of 1-methoxy-2-propanol was added to a 1000 mL three-necked flask, and heated to 85° C. under a nitrogen stream. A solution of 63.4 g of benzyl methacrylate, 72.3 g of methacrylic acid, and 4.15 g of V-601 (Wako Pure Chemicals) was added dropwise thereto in 159 g of 1-methoxy-2-propanol over 2 hours. After completion of the dropwise addition, it was heated for 5 hours to make it react. Next, heating was stopped to obtain a copolymer of benzyl methacrylate / methacrylic acid (30 / 70 mol% ratio).
[0730] Next, 120.0 g of the above-mentioned copolymer solution was transferred to a 300 mL three-necked flask, 16.6 g of glycidyl methacrylate and 0.16 g of p-methoxyphenol were added, and stirred to dissolve. After dissolution, 3.0 g of triphenylphosphine was added, heated to 100° C., and addition reaction was carried out. After confirming the disappearance of glycidyl methacrylate by gas chromatography, heating was stopped. 1-Methoxy-2-propanol was added to prepare a so...
Synthetic example 2~27
[0735] In order to obtain the desired polymer compound, except that benzyl methacrylate, methacrylic acid and glycidyl methacrylate in Synthesis Example 1 are changed into suitable arbitrary monomers, the others are the same as Synthesis Example 1, and prepared respectively Polymer compounds 2 to 27 shown in Tables 1 to 5.
[0736] [Table 1]
[0737]
[0738] [Table 2]
[0739]
[0740] [table 3]
[0741]
[0742] [Table 4]
[0743]
[0744] [table 5]
[0745]
[0746] In Tables 1 to 5, *1 represents a mixture of the structure represented by the following structural formula (a) and the structure represented by (b) (the mixing ratio is unknown), and *2 represents the structure represented by the following structural formula (c) and ( d) Mixing (mixing ratio unknown).
[0747] [chem 34]
[0748] Structural formula (a)
[0749] Structural formula (b)
[0750] [chem 35]
[0751] Structural formula (c)
[0752] Structural formula (d)
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