An adhesive coating composition for dentistry
A technology of adhesion and primer, applied in dental preparations, dentistry, dental prosthesis, etc., can solve the problems of insufficient storage stability and adhesion durability, and achieve the effect of long-lasting adhesion durability
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Embodiment 1 to 6
[0242] Adhesion treatment (application of primer agent / stand for 10 seconds / dry / apply adhesive material / light irradiation for 10 seconds).
[0243] After a filling operation with a photopolymerizable composite resin (BEAUTIFIL, manufactured by SHOFU INC.), a dentin adhesion test, an adhesion durability test, and a storage stability test were conducted. The results are shown in Table 6.
[0244] It is evident from Table 6 that the adhesive system comprising the one-component primer compositions 1 to 6 has good dentin adhesiveness to enamel and dentin (after immersion in water at 37° C. for 24 hours). It was also found that the adhesive system comprising the one-liquid type primer compositions 1 to 6 has good adhesive durability because when compared with the adhesiveness of the dentin after immersion in water at 37° C. for 24 hours, with respect to the enamel Adhesion durability after about 2,000 thermal cycles of both the dentin and the adhesive strength does not decrease. ...
Embodiment 7 to 12
[0262] Adhesive treatment by a two-step type adhesive system comprising a combination of two-polymer two-liquid type adhesive material composition C or D and one-liquid type primer compositions 1 to 6 (primer application / stand for 10 seconds / dry / mix the bonding material in the same amount and apply). After a filling operation with a photopolymerizable composite resin (BEAUTIFIL, manufactured by SHOFU INC.), a dentin adhesion test, an adhesion durability test, and a storage stability test were conducted. The results are shown in Table 6.
[0263] It is evident from Table 6 that the one-component primer compositions 1 to 6 have good dentin adhesion to enamel and dentin even in the adhesive system comprising a dual polymeric adhesive material (immersion in 37 after 24 hours in water at °C). It was also found that the one-component type primer composition has good adhesion durability, because when compared with the adhesion to the dentin after immersion in water at 37° C. fo...
Embodiment 13 to 18
[0265] Adhesion treatment (primer application / standing for 10 seconds / drying / light irradiation for 10 seconds) was performed by a one-step adhesion system using one-liquid type primer compositions 1 to 6 alone, and The same tests as in Examples 1 to 6 were carried out. The results are shown in Table 6.
[0266] As is apparent from Table 6, the adhesive systems using the one-component primer compositions 1 to 6 alone showed: in any one of dentin adhesiveness, adhesive durability, and storage stability, enamel and dentin. Both were stable in adhesiveness, although at a low level compared with an adhesive system using a combination of a photopolymerizable one-component type and a double-polymerized two-component type adhesive material.
[0267] Table 6
[0268] Results of Adhesive Systems Including One-Component Primer Compositions in Various Tests
[0269]
[0270] Table 6 - continued -
[0271]
[0272] Table 6 - continued -
[0273]
[0274] Table 6 - continued -...
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