Preparation method of depolymerized and dispersed viscosity reducer of heavy oil
A viscosity reducing agent and depolymerization technology, applied in chemical instruments and methods, drilling compositions, etc., can solve the problems of limited degree of viscosity reduction and pour point reduction, disappearance, and reducing the application value of chemical viscosity reduction technology.
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[0019] A preparation method for a thick oil depolymerization dispersion viscosity reducer, which is actually a preparation method for a water-soluble cationic polymer, including selecting octadecyldimethyl tertiary amine as a hydrophobic group monomer, diethylene Triamine, epichlorohydrin, and benzyl chloride are hydrophilic group monomers, and ethanol is used as a solvent. It is characterized in that the sequence of specific steps is as follows:
[0020] (1) Add 0.35mol to 0.45mol of octadecyldimethyl tertiary amine and 0.7mol of ethanol into a reaction vessel with a stirring device, and mix it into a homogeneous solution at a stirring speed of 200r / min-400r / min, Place in a constant temperature jacket at 50°C to 70°C for 0.5 hours;
[0021] (2) Slowly add 0.30 mol to 0.45 mol of epichlorohydrin into the reaction vessel at a rate of 5.0 ml / min to 20 ml / min with a dropping funnel, and after the addition is completed, the temperature of the reaction solution is raised to 70°C-7...
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