Photocatalyst thin film, method for forming photocatalyst thin film, and photocatalyst thin film coated product
A technology of photocatalytic thin films and products, which is applied in the direction of catalyst activation/preparation, chemical instruments and methods, physical/chemical process catalysts, etc., and can solve problems such as poor wear resistance, low adhesion of glass and coating films, etc.
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[0053] The present invention will be described based on examples.
[0054] (a) Preparation of coating solution
[0055] Mix catechol in an appropriate amount of toluene, add ethoxylated niobium (V) (Niobium (V) ethoxide) dropwise to the resulting mixed solution, and make the moles of ethoxylated niobium (V) and catechol The ratio is 2:5. The total amount of solvent was adjusted so that the concentration of niobium (V) ethoxide was 0.5M.
[0056] Half of the solution was distilled off. During distillation, it was confirmed that the vapor temperature reached 100° C., and the volatile components of the mixed solution remaining after distillation were evaporated under reduced pressure using a rotary evaporator. The remaining solid components were then heated to 100° C. under vacuum using a vacuum dryer to completely remove the remaining volatile components. Drying was continued until a solid content (niobium catechol) was obtained in an amount close to the theoretical value (a...
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