Electrode for non-aqueous electrolyte secondary battery, manufacturing method therefor, and non-aqueous electrolyte secondary battery
A non-aqueous electrolyte and secondary battery technology, applied in non-aqueous electrolyte battery electrodes, electrode manufacturing, battery electrodes, etc., can solve the problem of insufficient filling rate of the mixture layer, and achieve the effect of excellent charge and discharge capacity
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Embodiment 1
[0107] (a) Preparation of positive electrode
[0108] "Cellseed N (trade name)" (lithium nickelate, LiNiO 2 ) 3 kg, 1 kg of "#1320 (trade name)" (NMP solution containing 12% by weight of PVDF) manufactured by Kureha Co., Ltd. as a positive electrode binder, 90 g of acetylene black as a conductive material, and an appropriate amount of NMP as a solvent ( N-methyl-2-pyrrolidone) is stirred with a double-arm type kneading machine, and is modulated into a positive electrode mixture paste.
[0109] The first active material particles had an average particle diameter (D50) of 11 μm and an average circularity of 0.97, and the compressive breaking strength of particles having a particle diameter of 11 μm and a circularity of 0.97 was 77 MPa.
[0110] The positive electrode mixture paste was applied to both sides of a 15-μm-thick aluminum foil as a positive electrode current collector except for the junction of the positive electrode lead, and dried to form a film. Then, the film was...
Embodiment 2
[0126] In order to increase the mechanical strength of the first active material particles, heating in an air atmosphere was performed at a temperature of 750° C. for 50 hours. As a result, the first active material particles had an average particle diameter of 11 μm and an average circularity of 0.99, and the compressive breaking strength of particles having a particle diameter of 11 μm and a circularity of 0.97 was 94 MPa. Furthermore, the interval between the rollers during compression was set to 70 μm to adjust the compressive stress, and control {(D 0 -D 1 ) / D 0}×100 is 20%. Except for this, a lithium ion secondary battery was produced in the same manner as in Example 1.
Embodiment 3
[0128] Set the interval between the rollers during compression to 20 μm to adjust the compressive stress, and control {(D 0 -D 1 ) / D 0}×100 is 40%. Except for this, a lithium ion secondary battery was produced in the same manner as in Example 2.
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