Method for synthesizing ordered mesoporous indium oxide
A synthesis method and indium oxide technology, applied in chemical instruments and methods, gallium/indium/thallium compounds, inorganic chemistry, etc., can solve the problem of lack of connection, poor connectivity of mesoporous silicon oxide, and inability to form mesoporous structures with interconnected skeletons etc. to achieve the effects of saving energy, high degree of order, and high degree of pore filling
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Embodiment 1
[0033] Mix 8.0g of surfactant P123, 60g of water and 240g of 2M hydrochloric acid at 35°C, stir for 1-12 hours until all the surfactants are dissolved and uniformly dispersed, then add 16.72g of ethyl orthosilicate TEOS, stir for 5 Minutes later, it was transferred to a polytetrafluoroethylene bottle and left to stand in an oven at 35°C for 20 hours, then hydrothermally reacted at 130°C for 1 day, cooled naturally, filtered with suction, washed, and dried naturally at room temperature to obtain a white powder.
[0034] Surfactant P123 was removed by solvent extraction: 1.0 g of the powder sample obtained above was added to 200 ml of ethanol (containing 16 ml of 36 wt% concentrated hydrochloric acid), stirred at 70° C. for 24 h in a reflux device, filtered, washed, and dried. The obtained ordered mesoporous silica has a specific surface area of 478m 2 / g, pore volume 1.00cm 3 / g, the Unicom pore size is greater than 4nm.
[0035] Take 0.6g of the above-mentioned treated mes...
Embodiment 2
[0037] Mix 8.0g of surfactant P123, 60g of water and 240g of 2M hydrochloric acid at 35°C, stir for 1-12 hours until all the surfactants are dissolved and uniformly dispersed, then add 16.72g of ethyl orthosilicate TEOS, stir for 5 Minutes later, it was transferred to a polytetrafluoroethylene bottle and left to stand in an oven at 35°C for 20 hours, followed by hydrothermal reaction at 130°C for 1 day, after natural cooling, suction filtration, washing, and natural drying at room temperature to obtain a white powder. Surfactant P123 was removed by solvent extraction: 1.0 g of the powder sample obtained above was added to 200 ml of ethanol (containing 16 ml of 36 wt% concentrated hydrochloric acid), stirred at 70° C. for 24 h in a reflux device, filtered, washed, and dried. The obtained ordered mesoporous silica has a specific surface area of 478m 2 / g, pore volume 1.00cm 3 / g, the Unicom pore size is greater than 4nm.
[0038] Use 0.6g of the above-mentioned treated mesop...
Embodiment 3
[0040] Mix 8.0g of surfactant P123, 60g of water and 240g of 2M hydrochloric acid at 35°C, stir for 1-12 hours until the surfactant is completely dissolved and dispersed evenly, then add 16.72g of ethyl orthosilicate TEOS, stir for 5 minutes , transferred to a polytetrafluoroethylene bottle and stood in an oven at 35°C for 20 hours, followed by hydrothermal reaction at 130°C for 5 days, natural cooling, suction filtration, washing, and natural drying at room temperature to obtain a white powder. Surfactant P123 was removed by solvent extraction: 1.0 g of the powder sample obtained above was added to 200 ml of ethanol (containing 16 ml of 36 wt% concentrated hydrochloric acid), stirred at 70° C. for 24 h in a reflux device, filtered, washed, and dried. The obtained ordered mesoporous silica has a specific surface area of 365m 2 / g, pore volume 1.21cm 3 / g, the Unicom pore size is greater than 8nm.
[0041] Use 0.6g of the above-mentioned treated mesoporous silica as a hard ...
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