Unlock instant, AI-driven research and patent intelligence for your innovation.

Acid-washing method for internal surfaces of metal capillary tubes

A capillary and surface acid technology, which is applied in the field of pickling of the inner surface of metal capillary materials, can solve the problems of enhanced liquid surface tension, inability to achieve pickling, and reduced surface area, and achieves simple processing, simple structure, and pickling. simple method effect

Active Publication Date: 2012-01-04
NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH
View PDF0 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] For pipes with an inner diameter of more than 2mm, the effect of surface tension is slight, and the acid liquid can flow smoothly in the pipe to realize the pickling process; but when the inner diameter of the pipe is less than 2mm, the effect of surface tension of the liquid is significantly enhanced, and it is difficult for the acid liquid to flow in the pipe , or cannot flow into the inside of the pipe, the reason is that when the acid liquid comes into contact with the gas inside the pipe, a surface layer will be formed, and the molecules in the surface layer of the liquid are sparser than the inside of the liquid, so they are subject to the force directed to the inside of the liquid, making The surface of the liquid has a tendency to shrink; at the same time, affected by the cohesive force between the liquid molecules, the liquid surface automatically shrinks, so that the acid liquid minimizes its surface area and does not flow into the capillary tube, making pickling impossible.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Acid-washing method for internal surfaces of metal capillary tubes
  • Acid-washing method for internal surfaces of metal capillary tubes
  • Acid-washing method for internal surfaces of metal capillary tubes

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0045] In this embodiment, the metal capillary tube material 1 to be pickled is pure titanium (TA2) and has a size of Φ1.8×0.2×200 mm, and when the tube is pickled, firstly, the pure titanium (TA2) material When carrying out pickling, the ratio is prepared to prepare the pickling solution. Here, the pickling solution prepared by uniformly mixing nitric acid, hydrofluoric acid and water with a volume ratio of 3:1:6 is selected; after that, a bunch of 60 TA2 After the lower end of the metal capillary bundle composed of pipes is fixed with sealing gasket 1, it is inserted vertically to the liquid surface of the pickling solution downward into the vertical pickling cylinder 3, and the bottom end of the TA2 pipe is connected to the vertical pickling cylinder 3. Keep the pickling liquid in contact with each other for 2-3 seconds, that is, after the pickling liquid used enters the inside of the TA2 pipe, use the pressure plate to continue pressing the pipe from top to bottom; The low...

Embodiment 2

[0048] In this embodiment, the metal capillary tube material 1 to be pickled is a magnesium alloy (AZ31) and its size is Φ2.0×0.3×100mm, firstly, the ratio of the magnesium alloy (AZ31) material to be pickled is prepared according to the routine Pickling solution, the pickling solution prepared by uniformly mixing oxalic acid and water with a weight ratio of 15:1000 is selected here; after that, the lower end of a bundle of metal capillary tubes composed of 40 AZ 31 pipes is sealed with a sealing gasket-2 After fixing, insert vertically to the liquid surface of the pickling liquid downward into the vertical pickling cylinder 3 until the bottom end of the AZ31 pipe is in contact with the pickling liquid contained in the vertical pickling cylinder 3, and keep it for 2-3 seconds, that is, After the pickling liquid used enters the inside of the AZ31 pipe, use the pressing plate to continue pressing the tube from top to bottom; in the process of pressing the tube, it should be ensur...

Embodiment 3

[0052] In this embodiment, the metal capillary tube material 1 to be pickled is a titanium alloy (TLM) tube with a size of Φ1.5×0.15×500 mm. A pickling solution, the pickling solution prepared by uniformly mixing nitric acid, hydrofluoric acid and water with a volume ratio of 4:1:5 is selected here; after that, the lower end of a bundle of metal capillary tubes composed of 100 TLM tubes is used After the sealing gasket 12 is fixed, insert it into the vertical pickling cylinder 3 perpendicular to the liquid surface of the pickling solution until the bottom end of the TLM pipe contacts the pickling solution contained in the vertical pickling cylinder 3, and keep it for 2 -3 seconds, that is, after the pickling liquid used enters the inside of the TLM tube, the pressure plate is used to continue pressing the tube from top to bottom; The surrounding outer walls are always in close contact with the inner wall of the vertical pickling cylinder 3, so that the pickling solution in the...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
thicknessaaaaaaaaaa
widthaaaaaaaaaa
Login to View More

Abstract

The invention discloses an acid-washing method for internal surfaces of metal capillary tubes, which comprises the following steps of: 1, the trimming and fixing of tubes to be acid-washed; 2, tube insertion; and 3, acid washing, wherein in the trimming and fixing of the tubes to be acid-washed, bottom ends of a plurality of upright metal capillary tubes to be acid-washed are aligned, and lower parts of the upright metal capillary tubes to be acid-washed are hooped tightly by a sealing washer 1 to form an upright metal capillary tube bundle; in the process of tube insertion, the sealing washer 1 is ensured to be always fixed to the lower part of the metal capillary tube bundle, and the peripheral outer wall of the metal capillary tube bundle is always in close contact with the inner wall of a vertical acid-washing cylinder; and in the acid washing process, after the plurality of metal capillary tubes to be acid-washed are immersed into acid-washing liquid completely, the acid-washing process of the internal surfaces of the metal capillary tubes to be acid-washed is completed by the conventional acid-washing method. The acid-washing method has the advantages of novel and reasonabledesign, low invested cost, simple acid-washing steps, convenient realization, good acid-washing effect and capability of realizing the acid-washing process of the metal capillary tubes of which the inner diameters are less than or equal to 2 millimeters simply and conveniently and realizing the acid-washing process of the internal surfaces of the plurality of metal capillary tubes at one time simultaneously.

Description

technical field [0001] The invention relates to a method for surface treatment of metal pipes, in particular to a method for pickling the inner surface of metal capillary pipes. Background technique [0002] Metal pipes generally need to undergo surface pickling during the production process or before the finished product leaves the factory. The pickling process in the pipe processing process is usually arranged before and after intermediate heat treatment (or annealing). Among them, the main purpose of pickling before heat treatment is to remove the oxide layer generated during processing, and at the same time play a role in degreasing; pickling after heat treatment is mainly used to remove the oxide layer generated in the heat treatment stage to avoid the presence of oxidation inclusions in subsequent processing Which affects the performance of the pipe. The finished pickling is generally bright pickling, the purpose is to improve the surface quality of the pipe. [0003...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C23G3/04
Inventor 皇甫强于振涛张亚峰袁思波尉北玲韩建业刘春潮刘少辉
Owner NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH