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Processing method of high-purity aloe acetylated polysaccharide

A technology of aloe acetylation and a processing method, which is applied in the processing field of aloe acetylated polysaccharide, can solve problems such as difficult aloe acetylated polysaccharide, and achieves the effects of maintaining cell vitality, improving body immunity, and highly resisting viral infection

Active Publication Date: 2012-05-23
YUNNAN TIANMEI TIANKANG BIOTECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the content of aloe acetylated polysaccharides obtained by existing aloe extraction and concentration processes can only reach about 3%, and it is difficult to obtain high-purity aloe acetylated polysaccharides with a content of more than 10%.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] A, after 30 tons of aloe leaves are peeled, broken and filtered, 13.5 tons of aloe juice and residue are obtained;

[0020] B, in step A gained 13.5 tons of aloe juice, add 675ml commercially available food grade pectinase (according to 50ml / 吨芦荟汁 ), then add 13.5 kg of commercially available food-grade activated carbon (according to 0.1% of the aloe juice quality), stir for enzymolysis and decolorization for 20 minutes, and then leave standstill until the aloe juice is clarified;

[0021] C, be that the microfiltration membrane of 10u carries out coarse filtration to the aloe clarified liquid of step B with filter aperture, obtains crude filtrate;

[0022] D, filter the crude filtrate of step C with a filter membrane with a filter aperture of 0.2u to obtain an aloe acetylated polysaccharide extract with a molecular weight cut-off of more than 1,000,000;

[0023] E, filter the ultrafiltration membrane with a filter aperture of 0.001u, filter the aloe acetylated polysac...

Embodiment 2

[0027] A, after 30 tons of aloe leaves are peeled, broken and filtered, 13.5 tons of aloe juice and surplus slag are obtained;

[0028] B, in step A gained 13.5 tons of aloe juice, add 945ml commercially available food grade pectinase (by 70ml / 吨芦荟汁 ), then add 40.5 kilograms of commercially available food-grade activated carbon (according to 0.3% of the aloe juice quality), stir for enzymolysis and decolorization for 40 minutes, and then leave standstill until the aloe juice is clarified;

[0029] C, be that the microfiltration membrane of 10u carries out coarse filtration to the aloe clarified liquid of step B with filter aperture, obtains crude filtrate;

[0030] D, filter the crude filtrate of step C with a filter membrane with a filter aperture of 0.2u to obtain an aloe acetylated polysaccharide extract with a molecular weight cut-off of more than 1,000,000;

[0031] E, filter the ultrafiltration membrane with a filter aperture of 0.001u, filter the aloe acetylated polys...

Embodiment 3

[0035] A, after 30 tons of aloe leaves are peeled, broken and filtered, 13.5 tons of aloe juice and surplus slag are obtained;

[0036] B, in step A gained 13.5 tons of aloe juice, add 810ml commercially available food grade pectinase (according to 60ml / 吨芦荟汁 ), then add 27 kilograms of commercially available food-grade activated carbon (according to 0.2% of the aloe juice quality), stir for enzymolysis and decolorization for 30 minutes, and leave standstill until the aloe juice is clarified;

[0037] C, be that the microfiltration membrane of 10u carries out coarse filtration to the aloe clarified liquid of step B with filter aperture, obtains crude filtrate;

[0038] D, filter the crude filtrate of step C with a filter membrane with a filter aperture of 0.2u to obtain an aloe acetylated polysaccharide extract with a molecular weight cut-off of more than 1,000,000;

[0039] E, filter the ultrafiltration membrane with a filter aperture of 0.001u, filter the aloe acetylated po...

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Abstract

The invention provides a processing method of high-purity aloe acetylated polysaccharide, comprising the steps of: peeling and crushing the aloe, filtering to obtain the aloe juice, adding the pectinase in the aloe juice according to the additive amount of 50-70 ml / ton of aloe juice, adding the active carbon in the aloe juice according to 0.1-0.3 of the mass of the aloe juice, then stirring for 20-40 min for enzymolysis and decolorization, and standing until the aloe juice is clear; thereafter, filtering by the microfiltration membrane with filtration aperture of 10 mu m, the filtration membrane with filtration aperture of 0.2 mu m and the ultrafiltration membrane with filtration aperture of 0.001 mu m, concentrating by the reverse osmosis membrane and drying to obtain the aloe powder, the mass content of the aloe acetylated polysaccharide reaches 15%. The invention realizes continuous separation at the normal temperature and enables various functional compositions in the aloe to be fully separated without adding any assistant, thereby the purity of the aloe acetylated polysaccharide is guaranteed and the extraction and separation costs are reduced.

Description

technical field [0001] The invention relates to a processing method of aloe acetylated polysaccharide, which belongs to the technical field of plant processing. Background technique [0002] In recent years, the United States has carried out more in-depth and detailed research on aloe polysaccharides. The research has confirmed that the ingredients in aloe polysaccharides that have anti-viral infection, anti-inflammatory, and bactericidal effects, maintain cell vitality, and improve body immunity are actually a kind of O-acetyl-containing glucomannan, commonly known as aloe acetylated glucomannan, referred to as aloe acetylated polysaccharides. The molecular weight distribution range of aloe acetylated polysaccharides is relatively small, ranging from 60,000 to 100,000. Under normal circumstances, the content of aloe acetylated polysaccharides in fresh leaves of aloe is extremely low, only 0.5‰~1‰, and the content of aloe acetylated polysaccharides in ordinary 200:1 aloe ge...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08B37/02C12S3/02
Inventor 罗秉俊
Owner YUNNAN TIANMEI TIANKANG BIOTECH CO LTD
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